trans,trans-(pentafluorophenyl)(PEt₃)2Pt(hexatriynediyl)Pt(PEt₃)2(p-tolyl)

Base Information

• Chemical Name: trans,trans-(pentafluorophenyl)(PEt₃)2Pt(hexatriynediyl)Pt(PEt₃)2(p-tolyl)
• CAS No.: 1070344-77-2
• Molecular Formula: C₄₃H₆₇F₅P₄Pt₂
• Molecular Weight: 1193.05

Synonyms:trans,trans-(pentafluorophenyl)(PEt₃)2Pt(hexatriynediyl)Pt(PEt₃)2(p-tolyl)

Chemical Property of trans,trans-(pentafluorophenyl)(PEt₃)2Pt(hexatriynediyl)Pt(PEt₃)2(p-tolyl)

Chemical Property:

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Technology Process of trans,trans-(pentafluorophenyl)(PEt₃)2Pt(hexatriynediyl)Pt(PEt₃)2(p-tolyl)

There total 1 articles about trans,trans-(pentafluorophenyl)(PEt₃)2Pt(hexatriynediyl)Pt(PEt₃)2(p-tolyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

trans-chlorobis(diethylphenylphosphine)(p-tolyl)platinum(II) + trans-(pentafluorophenyl)(PEt3)2Pt(triethylsilylhexatriynyl) (1021954-93-7) → trans,trans-(pentafluorophenyl)(PEt3)2Pt(hexatriynediyl)Pt(PEt3)2(p-tolyl) (1070344-77-2)

Guidance literature:

With t-BuOK; KPF₆; n-Bu₄NF; copper(l) chloride; In tetrahydrofuran; methanol; dichloromethane; using Schlenk techniques; n-Bu4NF in THF-H2O (5 wt%) added to Pt-C6SiEt3complex in CH2Cl2 with stirring, 15 min; mixt. of (p-tolyl)Pt(PEt3)2Cl, t-BuOK, KPF6, CuCl, THF and MeOH added; stirred overnight; filtered; ppt. washed with EtOH; dried in vac.; elem. anal.;

DOI:10.1021/om800493x

upstream raw materials:

trans-(pentafluorophenyl)(PEt₃)2Pt(triethylsilylhexatriynyl)

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