C₅₂H₆₀N₆O₈

Base Information

Chemical Name:C₅₂H₆₀N₆O₈
CAS No.:1601496-83-6
Molecular Formula:C₅₂H₆₀N₆O₈
Molecular Weight:897.084
Hs Code.:

C<sub>52</sub>H<sub>60</sub>N<sub>6</sub>O<sub>8</sub>

Synonyms:C₅₂H₆₀N₆O₈

Suppliers and Price of C₅₂H₆₀N₆O₈

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₂H₆₀N₆O₈

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₂H₆₀N₆O₈

There total 12 articles about C₅₂H₆₀N₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1601495-49-1
C₉H₁₂O

: C₄₃H₄₈N₆O₇

: 1601496-83-6
C₅₂H₆₀N₆O₈

Guidance literature:: C₄₃H₄₈N₆O₇; With lithium aluminium tetrahydride; In tetrahydrofuran; at -78 - 0 ℃; for 1h;

C₉H₁₂O; In tetrahydrofuran; at -78 ℃; for 2.5h;
DOI:10.1002/anie.201308017

Reference yield:

: 79482-35-2
9-Hydroxy-8-methoxy-3-methyl-3,4-dihydro-2H-anthracen-1-one

: 1601496-83-6
C₅₂H₆₀N₆O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron tribromide / dichloromethane / 6.5 h / -78 - -20 °C

2.1: calcium sulfate; scandium tris(trifluoromethanesulfonate) / 1,2-dichloro-ethane / 2.5 h / -30 - -10 °C / Inert atmosphere

3.1: calcium sulfate; scandium tris(trifluoromethanesulfonate) / 1,2-dichloro-ethane / 20 h / -30 - 28 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.67 h / 0 °C

4.2: 5 h / 0 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -78 - 0 °C

5.2: 2.5 h / -78 °C

With calcium sulfate; lithium aluminium tetrahydride; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium hydride; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/anie.201308017

Reference yield:

: 1601495-45-7
C₇H₁₄O

: 1601496-83-6
C₅₂H₆₀N₆O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methylmorpholine N-oxide; tetra-n-propylammonium perruthenate. / dichloromethane / 1 h / 0 - 20 °C / Molecular sieve

2.1: zinc; triphenylphosphine / dichloromethane / 1 h / 0 - 20 °C

2.2: 0.5 h / 0 - 20 °C

3.1: n-butyllithium / hexane / 2 h / -78 - 0 °C

3.2: 2.5 h / -78 - 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -78 - 0 °C

4.2: 2.5 h / -78 °C

With lithium aluminium tetrahydride; n-butyllithium; tetra-n-propylammonium perruthenate.; 4-methylmorpholine N-oxide; triphenylphosphine; zinc; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/anie.201308017