12-nitro-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Base Information

Chemical Name:12-nitro-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone
CAS No.:1415684-66-0
Molecular Formula:C₃₅H₃₄Cl₄N₄O₆S
Molecular Weight:780.556
Hs Code.:

Synonyms:12-nitro-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

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Chemical Property of 12-nitro-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

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Technology Process of 12-nitro-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

There total 4 articles about 12-nitro-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1415684-62-6
12-nitro-7-oxo-N,N-(tetrachlorophthaloyl)dehydroabietylamine

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1415684-66-0
12-nitro-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; benzene; for 8h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2012.10.071

Reference yield:

: 117-08-8
tetrachlorophthalic anhydride

: 1415684-66-0
12-nitro-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 2.5 h / 130 °C / Inert atmosphere

2.1: acetic anhydride

2.2: 25 h / 20 °C

3.1: toluene-4-sulfonic acid / benzene; ethanol / 8 h / Reflux; Inert atmosphere

With acetic anhydride; toluene-4-sulfonic acid; acetic acid; In ethanol; benzene;
DOI:10.1016/j.tet.2012.10.071

Reference yield:

: 1384983-06-5
N,N-(tetrachlorophthaloyl)dehydroabietylamine

: 1415684-66-0
12-nitro-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride

1.2: 25 h / 20 °C

2.1: toluene-4-sulfonic acid / benzene; ethanol / 8 h / Reflux; Inert atmosphere

With acetic anhydride; toluene-4-sulfonic acid; In ethanol; benzene;
DOI:10.1016/j.tet.2012.10.071