N-[2-cyanoethyl(phenyl)phosphinothioyl]-L-glutamic acid dimethyl ester

Base Information

Chemical Name:N-[2-cyanoethyl(phenyl)phosphinothioyl]-L-glutamic acid dimethyl ester
CAS No.:253269-37-3
Molecular Formula:C₁₆H₂₁N₂O₅PS
Molecular Weight:384.393
Hs Code.:

Synonyms:N-[2-cyanoethyl(phenyl)phosphinothioyl]-L-glutamic acid dimethyl ester

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Chemical Property of N-[2-cyanoethyl(phenyl)phosphinothioyl]-L-glutamic acid dimethyl ester

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Technology Process of N-[2-cyanoethyl(phenyl)phosphinothioyl]-L-glutamic acid dimethyl ester

There total 5 articles about N-[2-cyanoethyl(phenyl)phosphinothioyl]-L-glutamic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 253269-39-5
N-[2-cyanoethyl(phenyl)phosphinyl]-L-glutamic acid dimethyl ester

: 253269-37-3
N-[2-cyanoethyl(phenyl)phosphinothioyl]-L-glutamic acid dimethyl ester

Guidance literature:: With Lawessons reagent;
DOI:10.1016/S0960-894X(99)00198-5

Reference yield:

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 253269-37-3
N-[2-cyanoethyl(phenyl)phosphinothioyl]-L-glutamic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole; diisopropylethylamine / benzene / 2 h / 4 - 20 °C

2: 0.43 g / diisopropylethylamine / benzene / 3 h / 20 °C

3: 1.12 g / Lawesson's reagent / toluene / 3 h / Heating

With Lawessons reagent; 1H-tetrazole; N-ethyl-N,N-diisopropylamine; In toluene; benzene; 1: Condensation / 2: Condensation / 3: Substitution;
DOI:10.1021/jo991090x

Reference yield:

: 66871-21-4
C₉H₉ClNO₂P

: 253269-37-3
N-[2-cyanoethyl(phenyl)phosphinothioyl]-L-glutamic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.43 g / diisopropylethylamine / benzene / 3 h / 20 °C

2: 1.12 g / Lawesson's reagent / toluene / 3 h / Heating

With Lawessons reagent; N-ethyl-N,N-diisopropylamine; In toluene; benzene; 1: Condensation / 2: Substitution;
DOI:10.1021/jo991090x