Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)*2CH₃OH=(Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆*2CH₃OH

Base Information

• Chemical Name: Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)*2CH₃OH=(Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆*2CH₃OH
• CAS No.: 87114-82-7
• Molecular Formula: 2CH₄O*C₃₆H₄₈ClFeN₆*F₆P
• Molecular Weight: 865.166

Synonyms:Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)*2CH₃OH=(Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆*2CH₃OH

Chemical Property of Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)*2CH₃OH=(Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆*2CH₃OH

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Technology Process of Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)*2CH₃OH=(Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆*2CH₃OH

There total 1 articles about Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)*2CH₃OH=(Cl(CH₂)6(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆*2CH₃OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

Fe(py)2Cl2 (15616-26-9) + H4(CH2)6(NCH3CC6H5C3HCH3N2(CH2)3)2(4+)*3PF6(1-)*Cl(1-)=(H4(CH2)6(NCH3CC6H5C3HCH3N2(CH2)3)2)(PF6)3Cl → Cl(CH2)6(NCH3CC6H5C3HCH3N2(CH2)3)2Fe(1+)*PF6(1-)*2CH3OH=(Cl(CH2)6(NCH3CC6H5C3HCH3N2(CH2)3)2Fe)PF6*2CH3OH (87114-82-7)

Guidance literature:

With triethylamine; In acetonitrile; ligand and slight excess of Fe complex slurring in MeCN, large excess of Et3N adding, refluxing for 5 min, cooling and filtering through celite, solvent removing, residue dissolving in hot MeOH, stirring for 10 min,filtering; purified by recrystn. from CH3CN/C2H5OH or MeOH; identified by elem. anal.;

DOI:10.1021/ja00360a008

upstream raw materials:

Fe(py)2Cl₂

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