1-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one

Base Information

Chemical Name:1-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one
CAS No.:75682-90-5
Molecular Formula:C₂₀H₂₆O₃
Molecular Weight:314.425
Hs Code.:

Synonyms:1-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one

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Chemical Property of 1-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one

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Technology Process of 1-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one

There total 6 articles about 1-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 75682-87-0
2-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-3-methyl-cyclohex-2-enone

: 75682-90-5
1-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In methanol; for 14h;

Reference yield:

: 87141-69-3
1-Cyclopropyl-3-(m-methoxyphenyl)propyl bromide

: 75682-90-5
1-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / ZnBr₂ / diethyl ether / 1.5 h / 0 °C

2: 86 percent / n-butyl lithium, HMPA / hexane; tetrahydrofuran / -78 °C

3: 75 percent / hydrogen peroxide, sodium hydroxide / methanol / 14 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; n-butyllithium; dihydrogen peroxide; zinc dibromide; In tetrahydrofuran; methanol; diethyl ether; hexane;

Reference yield:

: 344334-33-4
1-Cyclopropyl-3-(3-methoxy-phenyl)-propan-1-one

: 75682-90-5
1-[(E)-6-(3-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaBH₄, 2.) PBr₃, LiBr / 1.) ethanol, 2.) collidine, ether, -40 deg C

2: 56 percent / ZnBr₂ / diethyl ether / 1.5 h / 0 °C

3: 86 percent / n-butyl lithium, HMPA / hexane; tetrahydrofuran / -78 °C

4: 75 percent / hydrogen peroxide, sodium hydroxide / methanol / 14 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; sodium tetrahydroborate; n-butyllithium; dihydrogen peroxide; phosphorus tribromide; lithium bromide; zinc dibromide; In tetrahydrofuran; methanol; diethyl ether; hexane;