2-methoxycarbonyl-3-octanoyl-(benzyl-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine

Base Information

• Chemical Name: 2-methoxycarbonyl-3-octanoyl-(benzyl-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine
• CAS No.: 144741-66-2
• Molecular Formula: C₂₄H₃₅NO₈
• Molecular Weight: 465.544

Synonyms:2-methoxycarbonyl-3-octanoyl-(benzyl-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine

Chemical Property of 2-methoxycarbonyl-3-octanoyl-(benzyl-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine

Chemical Property:

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Technology Process of 2-methoxycarbonyl-3-octanoyl-(benzyl-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine

There total 3 articles about 2-methoxycarbonyl-3-octanoyl-(benzyl-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-methoxycarbonyl-3-octanoyl-(benzyl-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine (144741-53-7) → 2-methoxycarbonyl-3-octanoyl-(benzyl-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine (144741-66-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol; for 16h; under 2068.6 Torr; Ambient temperature;

DOI:10.1016/0008-6215(92)80057-8

Reference yield:

benzyl-4,6-O-benzylidene-2-deoxy-2-octanamido-α-D-glucopyranoside (102690-79-9) → 2-methoxycarbonyl-3-octanoyl-(benzyl-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine (144741-66-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 1) NaH / 1,4-dioxane, 1) 80 deg C, 15 min., 2) 80 deg C, 3 h

2: 91 percent / methanol

3: 96 percent / H₂ / 10percent Pd/C / methanol; dioxane / 16 h / 2068.6 Torr / Ambient temperature

With hydrogen; sodium hydride; palladium on activated charcoal; In 1,4-dioxane; methanol;

DOI:10.1016/0008-6215(92)80057-8

Reference yield:

2-carboxy-3-octanoyl-(benzyl-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine (144741-52-6) → 2-methoxycarbonyl-3-octanoyl-(benzyl-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine (144741-66-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / methanol

2: 96 percent / H₂ / 10percent Pd/C / methanol; dioxane / 16 h / 2068.6 Torr / Ambient temperature

With hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol;

DOI:10.1016/0008-6215(92)80057-8

upstream raw materials:

2-methoxycarbonyl-3-octanoyl-(benzyl-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine

benzyl-4,6-O-benzylidene-2-deoxy-2-octanamido-α-D-glucopyranoside

2-carboxy-3-octanoyl-(benzyl-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido)<2,3-d>oxazolidine

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