6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester

Base Information

Chemical Name:6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester
CAS No.:208047-77-2
Molecular Formula:C₄₇H₅₁NO₁₂
Molecular Weight:821.921
Hs Code.:

6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester

Synonyms:6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester

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Chemical Property of 6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester

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Technology Process of 6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester

There total 1 articles about 6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 6-(4-Hydroxymethyl-phenoxy)-hexanoic acid methyl ester

: 208047-70-5
3,6-di-O-benzyl-2-deoxy-4-O-levulinoyl-2-phthalimido-β-D-glucopyranosyl trichloroacetimidate

: 208047-77-2
6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1055/s-1998-1750

Reference yield: 89.0%

: 208047-77-2
6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester

: 6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid

Guidance literature:: With pyridine; hydrazine hydrate; acetic acid;
DOI:10.1055/s-1998-1750

Reference yield:

: 208047-77-2
6-{4-[(2R,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-5-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-yloxymethyl]-phenoxy}-hexanoic acid methyl ester

: 2-[(3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-2-hydroxy-5-((3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / H₂NNH₂*xH₂O, CH₃COOH, pyridine

With pyridine; hydrazine hydrate; acetic acid;
DOI:10.1055/s-1998-1750