C₄₃H₆₆O₈S₂Si

Base Information

Chemical Name:C₄₃H₆₆O₈S₂Si
CAS No.:918897-12-8
Molecular Formula:C₄₃H₆₆O₈S₂Si
Molecular Weight:803.21
Hs Code.:

C<sub>43</sub>H<sub>66</sub>O<sub>8</sub>S<sub>2</sub>Si

Synonyms:C₄₃H₆₆O₈S₂Si

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Chemical Property of C₄₃H₆₆O₈S₂Si

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Technology Process of C₄₃H₆₆O₈S₂Si

There total 18 articles about C₄₃H₆₆O₈S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 929075-06-9
C₃₉H₅₆O₉Si

: 5573-62-6
(ethylthio)trimethylsilane

: 918897-12-8
C₄₃H₆₆O₈S₂Si

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - -40 ℃;
DOI:10.1016/j.bmcl.2006.09.004

Reference yield:

: 918896-99-8
CH₃OC₇H₆O(HO₂C(CH₂)2)C₅H₆OCH₂OC₇H₇(OC₇H₇)

: 918897-12-8
C₄₃H₆₆O₈S₂Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: EDC*HCl; DMAP; CSA / CH₂Cl₂ / Heating

2.1: H₂O; TsOH / methanol / 20 °C

3.1: 2,6-lutidine / dimethylformamide / 0 °C

4.1: Cp₂Ti[P(OEt)3]2 / tetrahydrofuran / 20 °C

5.1: BH₃*THF / 0 - 20 °C

5.2: NaBO₃ / H₂O; tetrahydrofuran / Heating

6.1: 93 percent / Dess-Martin periodinane / CH₂Cl₂ / 20 °C

7.1: 63 percent / DDQ / H₂O; CH₂Cl₂ / 0 - 20 °C

8.1: 87 percent / TMSOTf / CH₂Cl₂ / -78 - -40 °C

With 2,6-dimethylpyridine; dmap; borane-THF; titanocene(II) triethylphosphite complex; trimethylsilyl trifluoromethanesulfonate; camphor-10-sulfonic acid; water; Dess-Martin periodane; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.09.004

Reference yield:

: 918897-20-8
C₃₅H₄₄O₇

: 918897-12-8
C₄₃H₆₆O₈S₂Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 97 percent / KOH / methanol; tetrahydrofuran; H₂O / Heating

2.1: EDC*HCl; DMAP; CSA / CH₂Cl₂ / Heating

3.1: H₂O; TsOH / methanol / 20 °C

4.1: 2,6-lutidine / dimethylformamide / 0 °C

5.1: Cp₂Ti[P(OEt)3]2 / tetrahydrofuran / 20 °C

6.1: BH₃*THF / 0 - 20 °C

6.2: NaBO₃ / H₂O; tetrahydrofuran / Heating

7.1: 93 percent / Dess-Martin periodinane / CH₂Cl₂ / 20 °C

8.1: 63 percent / DDQ / H₂O; CH₂Cl₂ / 0 - 20 °C

9.1: 87 percent / TMSOTf / CH₂Cl₂ / -78 - -40 °C

With 2,6-dimethylpyridine; dmap; potassium hydroxide; borane-THF; titanocene(II) triethylphosphite complex; trimethylsilyl trifluoromethanesulfonate; camphor-10-sulfonic acid; water; Dess-Martin periodane; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.09.004