2-<3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenylsalicyl>-4-phenylphenol

Base Information

Chemical Name:2-<3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenylsalicyl>-4-phenylphenol
CAS No.:81535-89-9
Molecular Formula:C₅₁H₃₉BrO₄
Molecular Weight:795.772
Hs Code.:

Synonyms:2-<3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenylsalicyl>-4-phenylphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenylsalicyl>-4-phenylphenol

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Technology Process of 2-<3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenylsalicyl>-4-phenylphenol

There total 7 articles about 2-<3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenylsalicyl>-4-phenylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 92-69-3
4-Phenylphenol

: 81535-88-8
3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol

: 81535-89-9
2-<3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenylsalicyl>-4-phenylphenol

Guidance literature:: With hydrogenchloride; In xylene; for 24h; Heating;
DOI:10.1021/jo00135a005

Reference yield:

: 92-69-3
4-Phenylphenol

: 81535-89-9
2-<3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenylsalicyl>-4-phenylphenol

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / bromine / CHCl₃ / 60 °C

2: 49 percent / KOH / H₂O / 72 h / 40 °C

3: 71 percent / conc. HCl / xylene / 20 h / Heating

4: 48 percent / KOH / H₂O / 144 h / 35 °C

5: 65 percent / conc. HCl / xylene / 20 h / Heating

6: 73 percent / KOH / H₂O / 144 h / Ambient temperature

7: 81 percent / conc. HCl / xylene / 24 h / Heating

With hydrogenchloride; potassium hydroxide; bromine; In chloroform; water; xylene;
DOI:10.1021/jo00135a005

Reference yield:

: 92-03-5
2-bromo-4-phenylphenol

: 81535-89-9
2-<3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenylsalicyl>-4-phenylphenol

Guidance literature:: Multi-step reaction with 6 steps

1: 49 percent / KOH / H₂O / 72 h / 40 °C

2: 71 percent / conc. HCl / xylene / 20 h / Heating

3: 48 percent / KOH / H₂O / 144 h / 35 °C

4: 65 percent / conc. HCl / xylene / 20 h / Heating

5: 73 percent / KOH / H₂O / 144 h / Ambient temperature

6: 81 percent / conc. HCl / xylene / 24 h / Heating

With hydrogenchloride; potassium hydroxide; In water; xylene;
DOI:10.1021/jo00135a005