(1R,3Z,6Z)-1-(hydroxymethyl)-3,6-nonadien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate

Base Information

Chemical Name:(1R,3Z,6Z)-1-(hydroxymethyl)-3,6-nonadien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate
CAS No.:1252798-86-9
Molecular Formula:C₃₆H₄₉IO₄Si
Molecular Weight:700.773
Hs Code.:

Synonyms:(1R,3Z,6Z)-1-(hydroxymethyl)-3,6-nonadien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate

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Chemical Property of (1R,3Z,6Z)-1-(hydroxymethyl)-3,6-nonadien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate

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Technology Process of (1R,3Z,6Z)-1-(hydroxymethyl)-3,6-nonadien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate

There total 1 articles about (1R,3Z,6Z)-1-(hydroxymethyl)-3,6-nonadien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1252798-61-0
(1R,3Z,6Z)-1-{[(4-methoxybenzyl)oxy]methyl}nona-3,6-dien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate

: 1252798-86-9
(1R,3Z,6Z)-1-(hydroxymethyl)-3,6-nonadien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201000565

Reference yield: 100.0%

: 1252798-86-9
(1R,3Z,6Z)-1-(hydroxymethyl)-3,6-nonadien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate

: 1252798-59-6
C₃₆H₄₇IO₄Si

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.201000565