sodium {3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethyldithiocarbamate

Base Information

Chemical Name:sodium {3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethyldithiocarbamate
CAS No.:1329562-98-2
Molecular Formula:C₁₇H₂₄NOS₃*Na
Molecular Weight:377.571
Hs Code.:

Synonyms:sodium {3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethyldithiocarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium {3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethyldithiocarbamate

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Technology Process of sodium {3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethyldithiocarbamate

There total 7 articles about sodium {3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethyldithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1329563-17-8
{3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethylamine

: 1329562-98-2
sodium {3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethyldithiocarbamate

Guidance literature:: With sodium methylate; In methanol; chloroform; at 20 ℃; for 2h;
DOI:10.1021/ja110244j

Reference yield:

: 1329563-52-1
N-{3-[4-(3-chloropropionyl)phenyl]propyl}acetamide

: 1329562-98-2
sodium {3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethyldithiocarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: triethylsilane / trifluoroacetic acid / 20 °C

2: dimethylsulfide borane complex / tetrahydrofuran; diethyl ether / 0 °C / Reflux

3: sodium iodide / N,N-dimethyl-formamide / 1.5 h / 20 °C

4: N,N-dimethyl-formamide / 20 °C

5: sodium methylate / methanol; chloroform / 2 h / 20 °C

With triethylsilane; dimethylsulfide borane complex; sodium methylate; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; chloroform; N,N-dimethyl-formamide; trifluoroacetic acid;
DOI:10.1021/ja110244j

Reference yield:

: 1329563-39-4
N-{3-[4-(3-chloropropyl)phenyl]propyl}acetamide

: 1329562-98-2
sodium {3-[4-(3-acetylsulfanylpropyl)phenyl]propyl}ethyldithiocarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylsulfide borane complex / tetrahydrofuran; diethyl ether / 0 °C / Reflux

2: sodium iodide / N,N-dimethyl-formamide / 1.5 h / 20 °C

3: N,N-dimethyl-formamide / 20 °C

4: sodium methylate / methanol; chloroform / 2 h / 20 °C

With dimethylsulfide borane complex; sodium methylate; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/ja110244j