(1R,3R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-1-hydroxy-6,7-methylenedioxy-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:(1R,3R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-1-hydroxy-6,7-methylenedioxy-1,2,3,4-tetrahydronaphthalene
CAS No.:1008303-67-0
Molecular Formula:C₂₁H₂₂O₇
Molecular Weight:386.401
Hs Code.:

Synonyms:(1R,3R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-1-hydroxy-6,7-methylenedioxy-1,2,3,4-tetrahydronaphthalene

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Chemical Property of (1R,3R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-1-hydroxy-6,7-methylenedioxy-1,2,3,4-tetrahydronaphthalene

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Technology Process of (1R,3R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-1-hydroxy-6,7-methylenedioxy-1,2,3,4-tetrahydronaphthalene

There total 4 articles about (1R,3R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-1-hydroxy-6,7-methylenedioxy-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1008303-61-4
(R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-6,7-methylenedioxy-1-oxo-1,2,3,4-tetrahydronaphthalene

: 1008303-67-0
(1R,3R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-1-hydroxy-6,7-methylenedioxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/adsc.200600632

Reference yield:

: 1008303-50-1
4,4-ethylenedioxy-6,7-methylenedioxy-1-oxo-1,4-dihydronaphthalene

: 1008303-67-0
(1R,3R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-1-hydroxy-6,7-methylenedioxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / (1R,4R)-2,5-diphenyl-bicyclo[2.2.2]octa-2,5-diene; aq. KOH / [RhCl(C₂H₄)2]2 / dioxane / 20 h / 20 °C

2: 94 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

With potassium hydroxide; lithium aluminium tetrahydride; bis(ethylene)rhodium(I) chloride dimer; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/adsc.200600632

Reference yield:

: 122775-35-3
3,4-Dimethoxyphenylboronic acid

: 1008303-67-0
(1R,3R)-3-(3,4-dimethoxyphenyl)-4,4-ethylenedioxy-1-hydroxy-6,7-methylenedioxy-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / (1R,4R)-2,5-diphenyl-bicyclo[2.2.2]octa-2,5-diene; aq. KOH / [RhCl(C₂H₄)2]2 / dioxane / 20 h / 20 °C

2: 94 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

With potassium hydroxide; lithium aluminium tetrahydride; bis(ethylene)rhodium(I) chloride dimer; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/adsc.200600632