5'-O-dimethoxytrityl-1-(2'-deoxy-β-D-ribofuranosyl)pyrrole-2-carbaldehyde

Base Information

Chemical Name:5'-O-dimethoxytrityl-1-(2'-deoxy-β-D-ribofuranosyl)pyrrole-2-carbaldehyde
CAS No.:540522-55-2
Molecular Formula:C₃₁H₃₁NO₆
Molecular Weight:513.59
Hs Code.:

Synonyms:5'-O-dimethoxytrityl-1-(2'-deoxy-β-D-ribofuranosyl)pyrrole-2-carbaldehyde

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Chemical Property of 5'-O-dimethoxytrityl-1-(2'-deoxy-β-D-ribofuranosyl)pyrrole-2-carbaldehyde

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Technology Process of 5'-O-dimethoxytrityl-1-(2'-deoxy-β-D-ribofuranosyl)pyrrole-2-carbaldehyde

There total 4 articles about 5'-O-dimethoxytrityl-1-(2'-deoxy-β-D-ribofuranosyl)pyrrole-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 540522-54-1
1-(2'-deoxy-β-D-ribofuranosyl)-pyrrole-2-carbaldehyde

: 540522-55-2
5'-O-dimethoxytrityl-1-(2'-deoxy-β-D-ribofuranosyl)pyrrole-2-carbaldehyde

Guidance literature:: With pyridine; at 20 ℃; for 4h;
DOI:10.1021/ja028806h

Reference yield:

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 540522-55-2
5'-O-dimethoxytrityl-1-(2'-deoxy-β-D-ribofuranosyl)pyrrole-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / acetonitrile / 1 h / 20 °C

1.2: 60 percent / acetonitrile / 1 h / 20 °C

2.1: 74 percent / NH₃ / methanol / 20 °C

3.1: 99 percent / pyridine / 4 h / 20 °C

With pyridine; ammonia; sodium hydride; In methanol; acetonitrile;
DOI:10.1021/ja028806h

Reference yield:

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 540522-55-2
5'-O-dimethoxytrityl-1-(2'-deoxy-β-D-ribofuranosyl)pyrrole-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / acetonitrile / 1 h / 20 °C

1.2: 60 percent / acetonitrile / 1 h / 20 °C

2.1: 74 percent / NH₃ / methanol / 20 °C

3.1: 99 percent / pyridine / 4 h / 20 °C

With pyridine; ammonia; sodium hydride; In methanol; acetonitrile;
DOI:10.1021/ja028806h