methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-α-D-arabino-hexopyranoside

Base Information

Chemical Name:methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-α-D-arabino-hexopyranoside
CAS No.:65827-68-1
Molecular Formula:C₁₇H₂₂BrNO₅
Molecular Weight:400.269
Hs Code.:

Synonyms:methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-α-D-arabino-hexopyranoside

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Chemical Property of methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-α-D-arabino-hexopyranoside

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Technology Process of methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-α-D-arabino-hexopyranoside

There total 6 articles about methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 65827-67-0,71695-37-9,72244-37-2,98758-30-6
methyl 3-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-methyl-α-D-arabino-hexopyranoside

: 65827-68-1
methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-α-D-arabino-hexopyranoside

Guidance literature:: With N-Bromosuccinimide; barium carbonate; In tetrachloromethane; for 4.5h; Heating;

Reference yield:

: 65827-65-8,71829-71-5
O^4',O^6'-(R)-benzylidene-O^1'-methyl-spiro[aziridine-2,3'-(α-D-arabino-2,3-dideoxy-hexopyranose)]

: 65827-68-1
methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 0.47 g / hydrogen / Raney nickel / methanol / 16 h / 15200 Torr / Ambient temperature

2: 41 percent / pyridine / 12 h / Ambient temperature

3: 86 percent / N-bromosuccinimide, barium carbonate / CCl₄ / 4.5 h / Heating

With N-Bromosuccinimide; hydrogen; barium carbonate; nickel; In pyridine; methanol; tetrachloromethane;

Reference yield:

: 63803-49-6
methyl 4,6-O-benzylidene-2,3-dideoxy-3-C-methylene-α-D-erythro-hexopyranoside

: 65827-68-1
methyl 3-acetamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-3-C-methyl-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 24 percent / iodine azide / acetonitrile

2: 0.7 g / lithium aluminium hydride / diethyl ether

3: 0.47 g / hydrogen / Raney nickel / methanol / 16 h / 15200 Torr / Ambient temperature

4: 41 percent / pyridine / 12 h / Ambient temperature

5: 86 percent / N-bromosuccinimide, barium carbonate / CCl₄ / 4.5 h / Heating

With N-Bromosuccinimide; lithium aluminium tetrahydride; iodine(I) azide; hydrogen; barium carbonate; nickel; In pyridine; methanol; tetrachloromethane; diethyl ether; acetonitrile;