(E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-N-methoxy-N-methylethanamide

Base Information

Chemical Name:(E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-N-methoxy-N-methylethanamide
CAS No.:1233405-30-5
Molecular Formula:C₁₈H₃₅NO₃Si
Molecular Weight:341.566
Hs Code.:

Synonyms:(E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-N-methoxy-N-methylethanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-N-methoxy-N-methylethanamide

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Technology Process of (E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-N-methoxy-N-methylethanamide

There total 1 articles about (E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-N-methoxy-N-methylethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 134833-70-8
dimethyl [2-(methoxy(methyl)amino)-2-oxoethyl]phosphonate

: 1233405-09-8
2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexanone

: 1233405-30-5
(E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-N-methoxy-N-methylethanamide

Guidance literature:: dimethyl [2-(methoxy(methyl)amino)-2-oxoethyl]phosphonate; With sodium hydride; In diethyl ether; mineral oil; at 0 ℃; Inert atmosphere;

2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexanone; In diethyl ether; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol101025r

Reference yield:

: 1233405-30-5
(E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-N-methoxy-N-methylethanamide

: 3727-48-8
2-bromocyclohexa-1,3-diene

: 1233405-12-3
(E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-1-(cyclohexa-1,5-dienyl)ethanone

Guidance literature:: 2-bromocyclohexa-1,3-diene; With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

(E)-2-(2-(tert-butyldimethylsilyloxy)-5,5-dimethylcyclohexylidene)-N-methoxy-N-methylethanamide; In tetrahydrofuran; at -78 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/ol101025r