14-[(⁽²⁾H₃)methyl]bicyclo[9.4.0]pentadec-1⁽¹¹⁾-en-12-one para-toluenesulfonylhydrazone

Base Information

• Chemical Name: 14-[(⁽²⁾H₃)methyl]bicyclo[9.4.0]pentadec-1⁽¹¹⁾-en-12-one para-toluenesulfonylhydrazone
• CAS No.: 1197240-89-3
• Molecular Formula: C₂₃H₃₄N₂O₂S
• Molecular Weight: 405.577

Synonyms:14-[(⁽²⁾H₃)methyl]bicyclo[9.4.0]pentadec-1⁽¹¹⁾-en-12-one para-toluenesulfonylhydrazone

Chemical Property of 14-[(⁽²⁾H₃)methyl]bicyclo[9.4.0]pentadec-1⁽¹¹⁾-en-12-one para-toluenesulfonylhydrazone

Chemical Property:

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Technology Process of 14-[(⁽²⁾H₃)methyl]bicyclo[9.4.0]pentadec-1⁽¹¹⁾-en-12-one para-toluenesulfonylhydrazone

There total 1 articles about 14-[(⁽²⁾H₃)methyl]bicyclo[9.4.0]pentadec-1⁽¹¹⁾-en-12-one para-toluenesulfonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

14-[((2)H3)methyl]bicyclo[9.4.0]pentadec-1(11)-en-12-one (1197240-73-5) + toluene-4-sulfonic acid hydrazide (1576-35-8) → 14-[((2)H3)methyl]bicyclo[9.4.0]pentadec-1(11)-en-12-one para-toluenesulfonylhydrazone (1197240-89-3)

Guidance literature:

With acetic acid; In methanol; at 64 ℃; for 5h;

DOI:10.1002/hlca.200900076

upstream raw materials:

14-[(⁽²⁾H₃)methyl]bicyclo[9.4.0]pentadec-1⁽¹¹⁾-en-12-one

toluene-4-sulfonic acid hydrazide

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