9-(4-chlorophenyl)-10-cyano-3-iodomethyl-2,3,5,6,7,8-hexahydrothiazolo<3,2-a>quinoline triiodide

Base Information

Chemical Name:9-(4-chlorophenyl)-10-cyano-3-iodomethyl-2,3,5,6,7,8-hexahydrothiazolo<3,2-a>quinoline triiodide
CAS No.:140424-41-5
Molecular Formula:C₁₉H₁₇ClIN₂S*I₃
Molecular Weight:848.494
Hs Code.:

Synonyms:9-(4-chlorophenyl)-10-cyano-3-iodomethyl-2,3,5,6,7,8-hexahydrothiazolo<3,2-a>quinoline triiodide

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Chemical Property of 9-(4-chlorophenyl)-10-cyano-3-iodomethyl-2,3,5,6,7,8-hexahydrothiazolo<3,2-a>quinoline triiodide

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Technology Process of 9-(4-chlorophenyl)-10-cyano-3-iodomethyl-2,3,5,6,7,8-hexahydrothiazolo<3,2-a>quinoline triiodide

There total 2 articles about 9-(4-chlorophenyl)-10-cyano-3-iodomethyl-2,3,5,6,7,8-hexahydrothiazolo<3,2-a>quinoline triiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 140709-01-9
2-allylthio-4-(4-chlorophenyl)-3-cyano-5,6,7,8-tetrahydroquinoline

: 140424-41-5
9-(4-chlorophenyl)-10-cyano-3-iodomethyl-2,3,5,6,7,8-hexahydrothiazolo<3,2-a>quinoline triiodide

Guidance literature:: With iodine; In chloroform; at 25 ℃; for 3h;

Reference yield:

: 83236-51-5
4-(4-chlorophenyl)-2-thioxo-1,2,5,6,7,8-hexahydroquinoline-3-carbonitrile

: 140424-41-5
9-(4-chlorophenyl)-10-cyano-3-iodomethyl-2,3,5,6,7,8-hexahydrothiazolo<3,2-a>quinoline triiodide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 10percent aq. KOH, DMF / 3 h / 25 °C

2: 78 percent / I₂ / CHCl₃ / 3 h / 25 °C

With potassium hydroxide; iodine; N,N-dimethyl-formamide; In chloroform;