[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]⁽¹⁺⁾*ClO₄^(1-)=[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]ClO₄

Base Information

• Chemical Name: [(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]⁽¹⁺⁾*ClO₄^(1-)=[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]ClO₄
• CAS No.: 85530-09-2
• Molecular Formula: C₄₂H₃₂Au₂N₄O₂P₂Rh*ClO₄
• Molecular Weight: 1282.98

Synonyms:[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]⁽¹⁺⁾*ClO₄^(1-)=[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]ClO₄

Chemical Property of [(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]⁽¹⁺⁾*ClO₄^(1-)=[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]ClO₄

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Technology Process of [(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]⁽¹⁺⁾*ClO₄^(1-)=[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]ClO₄

There total 2 articles about [(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]⁽¹⁺⁾*ClO₄^(1-)=[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)2]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

[(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(C8H12)](1+)*ClO4(1-)=[(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(C8H12)]ClO4 (85530-03-6) → [(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(CO)2](1+)*ClO4(1-)=[(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(CO)2]ClO4 (85530-09-2)

Guidance literature:

With CO; In dichloromethane; dry CO bubbled for 20 min through soln. of Rh complex in CH2Cl2 at 25°C; hexane added, concd., filtered, ppt. washed with Et2O and hexane, driedin vac.; elem. anal.;

DOI:10.1039/DT9830000323

Reference yield:

{(1,2-bis(diphenylphosphino)ethane)Au2}(μ-2,2'-bibenzimidazolato) (84076-81-3) → [(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(CO)2](1+)*ClO4(1-)=[(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(CO)2]ClO4 (85530-09-2)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: CO / dichloromethane

With CO; In dichloromethane; acetone;

DOI:10.1039/DT9830000323

Reference yield:

[(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(CO)2](1+)*ClO4(1-)=[(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(CO)2]ClO4 (85530-09-2) → [(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(CO)(P(C6H5)3)](1+)*ClO4(1-)=[(((C6H5)2PCH2)2)Au2(C14H8N4)Rh(CO)(P(C6H5)3)]ClO4 (85539-01-1)

Guidance literature:

With PPh₃; In dichloromethane; PPh3 added to soln. of heterobinuclear complex in CH2Cl2, stirred for 2h at 25°C; evapd., Et2O added, filtered, ppt. washed with Et2O, dried in vac.;

DOI:10.1039/DT9830000323

upstream raw materials:

[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(C₈H₁₂)]⁽¹⁺⁾*ClO₄^(1-)=[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(C₈H₁₂)]ClO₄

{(1,2-bis(diphenylphosphino)ethane)Au2}(μ-2,2'-bibenzimidazolato)

Downstream raw materials:

[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[(((C₆H₅)2PCH₂)2)Au₂(C₁₄H₈N₄)Rh(CO)(P(C₆H₅)3)]ClO₄

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