S-(N-<2-(2-phenyl-1-adamantyl)ethyl>carbamidinium)methyl hydrogen phosphorothioate

Base Information

Chemical Name:S-(N-<2-(2-phenyl-1-adamantyl)ethyl>carbamidinium)methyl hydrogen phosphorothioate
CAS No.:117077-39-1
Molecular Formula:C₂₀H₂₉N₂O₃PS
Molecular Weight:408.502
Hs Code.:

Synonyms:S-(N-<2-(2-phenyl-1-adamantyl)ethyl>carbamidinium)methyl hydrogen phosphorothioate

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Chemical Property of S-(N-<2-(2-phenyl-1-adamantyl)ethyl>carbamidinium)methyl hydrogen phosphorothioate

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Technology Process of S-(N-<2-(2-phenyl-1-adamantyl)ethyl>carbamidinium)methyl hydrogen phosphorothioate

There total 6 articles about S-(N-<2-(2-phenyl-1-adamantyl)ethyl>carbamidinium)methyl hydrogen phosphorothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 117077-29-9
N-<2-(2-phenyl-1-adamantyl)ethyl>-2-chloroacetamidine hydrochloride

: 117077-39-1
S-(N-<2-(2-phenyl-1-adamantyl)ethyl>carbamidinium)methyl hydrogen phosphorothioate

Guidance literature:: With hydrogenchloride; trisodium thiophosphate; In ethanol; water; for 0.5h;
DOI:10.1016/S0040-4020(01)90332-1

Reference yield:

: 117077-56-2
1-Bromomethyl-2-phenyl-adamantane

: 117077-39-1
S-(N-<2-(2-phenyl-1-adamantyl)ethyl>carbamidinium)methyl hydrogen phosphorothioate

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / dimethylsulfoxide / 15 h / 80 - 100 °C

2: 79 percent / 30 percent H₂O₂, 0.2 M aq. NaOH / methanol; dimethylsulfoxide / 12 h / 50 - 55 °C

3: 87 percent / 1.) LiAlH₄ 2.) HCl gas / tetrahydrofuran / 24 h / Heating

4: 87 percent / HCl / methanol / 12 h

5: 91 percent / 1.) trisodium phosphorothioate 2.) 6 N HCl / ethanol; H₂O / 0.5 h

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; dihydrogen peroxide; trisodium thiophosphate; In tetrahydrofuran; methanol; ethanol; water; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(01)90332-1

Reference yield:

: 117077-13-1
1-(cyanomethyl)-2-phenyladamantane

: 117077-39-1
S-(N-<2-(2-phenyl-1-adamantyl)ethyl>carbamidinium)methyl hydrogen phosphorothioate

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / 30 percent H₂O₂, 0.2 M aq. NaOH / methanol; dimethylsulfoxide / 12 h / 50 - 55 °C

2: 87 percent / 1.) LiAlH₄ 2.) HCl gas / tetrahydrofuran / 24 h / Heating

3: 87 percent / HCl / methanol / 12 h

4: 91 percent / 1.) trisodium phosphorothioate 2.) 6 N HCl / ethanol; H₂O / 0.5 h

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; dihydrogen peroxide; trisodium thiophosphate; In tetrahydrofuran; methanol; ethanol; water; dimethyl sulfoxide;
DOI:10.1016/S0040-4020(01)90332-1