Technology Process of (E)-2',6'-dimethoxystyryl-6-methoxy-3-aminobenzylsulfone
There total 5 articles about (E)-2',6'-dimethoxystyryl-6-methoxy-3-aminobenzylsulfone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium dithionite;
In
water; acetone;
at 50 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jm200570p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetic acid; benzylamine / Inert atmosphere; Reflux
2: sodium dithionite / water; acetone / 1 h / 50 °C / Inert atmosphere
With
sodium dithionite; acetic acid; benzylamine;
In
water; acetone;
1: Knoevenagel condensation / 2: Knoevenagel condensation;
DOI:10.1021/jm200570p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / methanol / 3 h / 20 °C / Inert atmosphere
2: dihydrogen peroxide; acetic acid / water / 24 h / 20 °C / Inert atmosphere
3: acetic acid; benzylamine / Inert atmosphere; Reflux
4: sodium dithionite / water; acetone / 1 h / 50 °C / Inert atmosphere
With
sodium dithionite; dihydrogen peroxide; acetic acid; benzylamine; sodium hydroxide;
In
methanol; water; acetone;
3: Knoevenagel condensation / 4: Knoevenagel condensation;
DOI:10.1021/jm200570p
