(E)-2-((2,4-dimethoxybenzyl)(2-((2,4-dimethoxybenzyl)(methyl)-amino)ethyl)amino)-1-phenylethanone oxime

Base Information

• Chemical Name: (E)-2-((2,4-dimethoxybenzyl)(2-((2,4-dimethoxybenzyl)(methyl)-amino)ethyl)amino)-1-phenylethanone oxime
• CAS No.: 1429769-51-6
• Molecular Formula: C₂₉H₃₇N₃O₅
• Molecular Weight: 507.63

Synonyms:(E)-2-((2,4-dimethoxybenzyl)(2-((2,4-dimethoxybenzyl)(methyl)-amino)ethyl)amino)-1-phenylethanone oxime

Chemical Property of (E)-2-((2,4-dimethoxybenzyl)(2-((2,4-dimethoxybenzyl)(methyl)-amino)ethyl)amino)-1-phenylethanone oxime

Chemical Property:

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Technology Process of (E)-2-((2,4-dimethoxybenzyl)(2-((2,4-dimethoxybenzyl)(methyl)-amino)ethyl)amino)-1-phenylethanone oxime

There total 3 articles about (E)-2-((2,4-dimethoxybenzyl)(2-((2,4-dimethoxybenzyl)(methyl)-amino)ethyl)amino)-1-phenylethanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1,4-bis(2,4-dimethoxybenzyl)-6-nitro-6-phenyl-1,4-diazepane (1416732-07-4) → (E)-2-((2,4-dimethoxybenzyl)(2-((2,4-dimethoxybenzyl)(methyl)-amino)ethyl)amino)-1-phenylethanone oxime (1429769-51-6)

Guidance literature:

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; at 20 ℃; Reagent/catalyst; Cooling with ice;

DOI:10.1039/c3ob40287h

Reference yield:

N1,N2-bis(2,4-dimethoxybenzyl)ethane-1,2-diamine → (E)-2-((2,4-dimethoxybenzyl)(2-((2,4-dimethoxybenzyl)(methyl)-amino)ethyl)amino)-1-phenylethanone oxime (1429769-51-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 80 °C

2: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol / 20 °C / Cooling with ice

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; ethanol; 1: |Mannich Aminomethylation;

DOI:10.1039/c3ob40287h

Reference yield:

1-nitro-1-phenylmethane (622-42-4) → (E)-2-((2,4-dimethoxybenzyl)(2-((2,4-dimethoxybenzyl)(methyl)-amino)ethyl)amino)-1-phenylethanone oxime (1429769-51-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 80 °C

2: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol / 20 °C / Cooling with ice

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; ethanol; 1: |Mannich Aminomethylation;

DOI:10.1039/c3ob40287h

upstream raw materials:

1,4-bis(2,4-dimethoxybenzyl)-6-nitro-6-phenyl-1,4-diazepane

1-nitro-1-phenylmethane

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