methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate

Base Information

Chemical Name:methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate
CAS No.:148564-34-5
Molecular Formula:C₄₉H₄₄N₆O₃S
Molecular Weight:796.993
Hs Code.:

methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate

Synonyms:methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate

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Chemical Property of methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate

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Technology Process of methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate

There total 6 articles about methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1918-78-1
2-methylthiophene-3-carboxylic acid

: 148564-34-5
methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄

2: 75 percent / N-bromosuccinimide, α,α'-azoisobutyronitrile / CCl4 / 3 h / 70 °C

3: 1.) NaH, 2.) LiBr

With N-Bromosuccinimide; sulfuric acid; azobisisobutyronitrile; sodium hydride; lithium bromide; In tetrachloromethane;
DOI:10.1021/jm00024a008

Reference yield:

: 53562-51-9
2-methylthiophene-3-carboxylic acid methyl ester

: 148564-34-5
methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / N-bromosuccinimide, α,α'-azoisobutyronitrile / CCl4 / 3 h / 70 °C

2: 1.) NaH, 2.) LiBr

With N-Bromosuccinimide; azobisisobutyronitrile; sodium hydride; lithium bromide; In tetrachloromethane;
DOI:10.1021/jm00024a008

Reference yield:

: 39815-78-6
methyl 3-oxoheptanoate

: 148564-34-5
methyl 2-<<4-butyl-2-methyl-6-oxo-5-<<2'-<1-(triphenylmethyl)-1H-tetrazol-5-yl><1,1'-biphenyl>-4-yl>methyl>-1(6H)-pyrimidinyl>methyl>-3-thiophenecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / NaH / tetrahydrofuran / 10 h

2: 70 percent / CH₃ONa / methanol; dioxane / 20 h / Ambient temperature

3: 1.) NaH, 2.) LiBr

With sodium methylate; sodium hydride; lithium bromide; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1021/jm00024a008