tris[diisopropylphosphinomethyl]phenylsilane

Base Information

• Chemical Name: tris[diisopropylphosphinomethyl]phenylsilane
• CAS No.: 1609574-92-6
• Molecular Formula: C₂₇H₅₃P₃Si
• Molecular Weight: 498.725
• Mol file: 1609574-92-6.mol

Synonyms:tris[diisopropylphosphinomethyl]phenylsilane

Chemical Property of tris[diisopropylphosphinomethyl]phenylsilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of tris[diisopropylphosphinomethyl]phenylsilane

There total 1 articles about tris[diisopropylphosphinomethyl]phenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

(isopropyl)2PCH2Li (579444-77-2) + Phenyltrichlorosilane (98-13-5) → tris[diisopropylphosphinomethyl]phenylsilane (1609574-92-6)

Guidance literature:

In tetrahydrofuran; at -78 - 20 ℃; for 14h;

DOI:10.1002/ejic.201301074

Reference yield: 85.0%

tris[diisopropylphosphinomethyl]phenylsilane (1609574-92-6) + iron(II) chloride → C27H53Cl2FeP3Si (1609574-94-8)

Guidance literature:

In tetrahydrofuran;

DOI:10.1002/ejic.201301074

Reference yield: 83.0%

C8H12Br2Os (900184-89-6) + tris[diisopropylphosphinomethyl]phenylsilane (1609574-92-6) → C54H106Br3Os2P6Si2(1+)*Br(1-)

Guidance literature:

In toluene; at 125 ℃;

DOI:10.1002/ejic.201301074

upstream raw materials:

(isopropyl)2PCH₂Li

Phenyltrichlorosilane

Downstream raw materials:

C₂₇H₅₃Cl₂FeP₃Si