1-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-4-methoxy-phenyl)-propane-1,3-dione

Base Information

Chemical Name:1-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-4-methoxy-phenyl)-propane-1,3-dione
CAS No.:692283-33-3
Molecular Formula:C₁₈H₁₈O₆
Molecular Weight:330.337
Hs Code.:

Synonyms:1-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-4-methoxy-phenyl)-propane-1,3-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-4-methoxy-phenyl)-propane-1,3-dione

Chemical Property:

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Technology Process of 1-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-4-methoxy-phenyl)-propane-1,3-dione

There total 6 articles about 1-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-4-methoxy-phenyl)-propane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101790-76-5
3,4-dimethoxy-benzoic acid-(2-acetyl-5-methoxy-phenyl ester)

: 692283-33-3
1-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-4-methoxy-phenyl)-propane-1,3-dione

Guidance literature:: With sodium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.5h;
DOI:10.1002/ejoc.201501278

Reference yield:

: 552-41-0
1-(2-hydroxy-4-methoxyphenyl)ethanone

: 692283-33-3
1-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-4-methoxy-phenyl)-propane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide / dichloromethane / 20 °C

2: sodium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C

With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; sodium hydroxide; In dichloromethane; dimethyl sulfoxide; 2: |Baker-Venkataraman Rearrangement;
DOI:10.1002/ejoc.201501278

Reference yield:

: 93-07-2
Veratric acid

: 692283-33-3
1-(3,4-dimethoxy-phenyl)-3-(2-hydroxy-4-methoxy-phenyl)-propane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide / dichloromethane / 20 °C

2: sodium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C

With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; sodium hydroxide; In dichloromethane; dimethyl sulfoxide; 2: |Baker-Venkataraman Rearrangement;
DOI:10.1002/ejoc.201501278