{1,1,1-trifluoro-2-[4-(1-methylethyl)phenyl]pent-4-ene-2-ylsulfonyl}benzene

Base Information

Chemical Name:{1,1,1-trifluoro-2-[4-(1-methylethyl)phenyl]pent-4-ene-2-ylsulfonyl}benzene
CAS No.:1402748-72-4
Molecular Formula:C₂₀H₂₁F₃O₂S
Molecular Weight:382.447
Hs Code.:

Synonyms:{1,1,1-trifluoro-2-[4-(1-methylethyl)phenyl]pent-4-ene-2-ylsulfonyl}benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {1,1,1-trifluoro-2-[4-(1-methylethyl)phenyl]pent-4-ene-2-ylsulfonyl}benzene

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Technology Process of {1,1,1-trifluoro-2-[4-(1-methylethyl)phenyl]pent-4-ene-2-ylsulfonyl}benzene

There total 2 articles about {1,1,1-trifluoro-2-[4-(1-methylethyl)phenyl]pent-4-ene-2-ylsulfonyl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1469-70-1
allyl ethyl carbonate

: 1402748-59-7
{2,2,2-trifluoro-1-[4-(1-methylethyl)phenyl]ethylsulfonyl}benzene

: 1402748-72-4
{1,1,1-trifluoro-2-[4-(1-methylethyl)phenyl]pent-4-ene-2-ylsulfonyl}benzene

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; at 20 - 40 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol302589w

Reference yield:

: 1402748-95-1
C₁₇H₁₇F₃S

: 1402748-72-4
{1,1,1-trifluoro-2-[4-(1-methylethyl)phenyl]pent-4-ene-2-ylsulfonyl}benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,2-bis-(diphenylphosphino)ethane / tetrahydrofuran / 1 h / 20 - 40 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 3-chloro-benzenecarboperoxoic acid; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol302589w