Gd⁽³⁺⁾*(CH₂CH₂NCH₂COO)3(CH₂CH₂NCH(COO)CH₂CH₂CON(CH₂)4NC₉H₅NCH₂OH)^(4-)=GdC₃₃H₄₃N₇O₁₀^(1-)

Base Information

• Chemical Name: Gd⁽³⁺⁾*(CH₂CH₂NCH₂COO)3(CH₂CH₂NCH(COO)CH₂CH₂CON(CH₂)4NC₉H₅NCH₂OH)^(4-)=GdC₃₃H₄₃N₇O₁₀^(1-)
• CAS No.: 1352640-91-5
• Molecular Formula: C₃₃H₄₃N₇O₁₀*Gd
• Molecular Weight: 854.995

Synonyms:Gd⁽³⁺⁾*(CH₂CH₂NCH₂COO)3(CH₂CH₂NCH(COO)CH₂CH₂CON(CH₂)4NC₉H₅NCH₂OH)^(4-)=GdC₃₃H₄₃N₇O₁₀^(1-)

Chemical Property of Gd⁽³⁺⁾*(CH₂CH₂NCH₂COO)3(CH₂CH₂NCH(COO)CH₂CH₂CON(CH₂)4NC₉H₅NCH₂OH)^(4-)=GdC₃₃H₄₃N₇O₁₀^(1-)

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Technology Process of Gd⁽³⁺⁾*(CH₂CH₂NCH₂COO)3(CH₂CH₂NCH(COO)CH₂CH₂CON(CH₂)4NC₉H₅NCH₂OH)^(4-)=GdC₃₃H₄₃N₇O₁₀^(1-)

There total 2 articles about Gd⁽³⁺⁾*(CH₂CH₂NCH₂COO)3(CH₂CH₂NCH(COO)CH₂CH₂CON(CH₂)4NC₉H₅NCH₂OH)^(4-)=GdC₃₃H₄₃N₇O₁₀^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Gd(III)-1,4,7,10-tetraazacyclododecane-1-glutaric acid-4,7,10-triacetic acid (1233956-56-3) + C23H25N3O2 (1352204-63-7) → Gd(3+)*(CH2CH2NCH2COO)3(CH2CH2NCH(COO)CH2CH2CON(CH2)4NC9H5NCH2OH)(4-)=GdC33H43N7O10(1-) (1352640-91-5) + 3-Phenylpropionic acid (501-52-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; water / 3 h / 20 °C

2: pH 7 / Aqueous TRIS buffer; X-irradiation

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water; N,N-dimethyl-formamide;

Reference yield:

Gd(3+)*(CH2CH2NCH2COO)3(CH2CH2NCH(COO)CH2CH2CON(CH2)4NC9H5NCH2OCOC2H4C6H5)(4-)=GdC42H51N7O11(1-) (1352640-87-9) → Gd(3+)*(CH2CH2NCH2COO)3(CH2CH2NCH(COO)CH2CH2CON(CH2)4NC9H5NCH2OH)(4-)=GdC33H43N7O10(1-) (1352640-91-5) + 3-Phenylpropionic acid (501-52-0)

Guidance literature:

pH=7; Quantum yield; Aqueous TRIS buffer; UV-irradiation;

upstream raw materials:

Gd(III)-1,4,7,10-tetraazacyclododecane-1-glutaric acid-4,7,10-triacetic acid

C₂₃H₂₅N₃O₂

Gd⁽³⁺⁾*(CH₂CH₂NCH₂COO)3(CH₂CH₂NCH(COO)CH₂CH₂CON(CH₂)4NC₉H₅NCH₂OCOC₂H₄C₆H₅)^(4-)=GdC₄₂H₅₁N₇O₁₁^(1-)

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