(R)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol

Base Information

Chemical Name:(R)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol
CAS No.:1417908-52-1
Molecular Formula:C₁₄H₂₂O₄
Molecular Weight:254.326
Hs Code.:

Synonyms:(R)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol

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Technology Process of (R)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol

There total 3 articles about (R)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: C₁₄H₂₀O₄

: 1417908-52-1
(R)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.5h; regioselective reaction;
DOI:10.1055/s-0032-1317346

Reference yield:

: 1053658-97-1
1-methoxy-4-(((4-methylpent-4-en-1-yl)oxy)methyl)benzene

: 1417908-52-1
(R)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol

: 1541193-60-5
(S)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol

Guidance literature:: With potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; (9S,9"S)-9,9"-[phthalazine-1,4-diylbis-(oxy)]bis[10,11-dihydro-6'-methoxycinchonane]; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 1h; Overall yield = 100 %; stereoselective reaction;
DOI:10.1055/s-0033-1340164

Reference yield:

: C₁₄H₂₀O₃

: 1417908-52-1
(R)-5-(4-methoxybenzyloxy)-2-methylpentane-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane / -20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; lithium aluminium tetrahydride; L-(+)-diisopropyl tartrate; In tetrahydrofuran; dichloromethane; 1: |Sharpless Asymmetric Epoxidation;
DOI:10.1055/s-0032-1317346