C₂₇H₂₆Cl₂N₂O₄

Base Information

Chemical Name:C₂₇H₂₆Cl₂N₂O₄
CAS No.:1309661-23-1
Molecular Formula:C₂₇H₂₆Cl₂N₂O₄
Molecular Weight:513.42
Hs Code.:

C<sub>27</sub>H<sub>26</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₇H₂₆Cl₂N₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₆Cl₂N₂O₄

Chemical Property:

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Technology Process of C₂₇H₂₆Cl₂N₂O₄

There total 6 articles about C₂₇H₂₆Cl₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72724-00-6
1-(benzyloxy)-4-(bromomethyl)-2-methoxybenzene

: 1309661-23-1
C₂₇H₂₆Cl₂N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide / tetrahydrofuran / 24 h / 60 °C

2: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C

3: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C

With tetrabutylammomium bromide; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201100495

Reference yield:

: 1309661-29-7
C₃₂H₃₀Cl₂O₆

: 1309661-23-1
C₂₇H₂₆Cl₂N₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C

2: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C

With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201100495

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 1309661-23-1
C₂₇H₂₆Cl₂N₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol / 2 h / 20 °C

2: phosphorus tribromide / dichloromethane / 0 - 20 °C

3: tetrabutylammomium bromide / tetrahydrofuran / 24 h / 60 °C

4: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C

5: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C

With sodium tetrahydroborate; tetrabutylammomium bromide; phosphorus tribromide; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201100495