{1-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-1,2,3-triazol-4-yl}methanol

Base Information

Chemical Name:{1-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-1,2,3-triazol-4-yl}methanol
CAS No.:1338831-30-3
Molecular Formula:C₁₃H₁₄N₆O
Molecular Weight:270.294
Hs Code.:

Synonyms:{1-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-1,2,3-triazol-4-yl}methanol

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Chemical Property of {1-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-1,2,3-triazol-4-yl}methanol

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Technology Process of {1-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-1,2,3-triazol-4-yl}methanol

There total 4 articles about {1-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-1,2,3-triazol-4-yl}methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1093981-03-3
4-(azidomethyl)-1-phenyl-1H-1,2,3-triazole

: 107-19-7
propargyl alcohol

: 1338831-30-3
{1-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-1,2,3-triazol-4-yl}methanol

Guidance literature:: With copper(II) acetate monohydrate; triphenylphosphine; In dichloromethane; at 20 ℃;
DOI:10.2478/s11532-013-0351-z

Reference yield: 51.0%

: 1338831-18-7
C₁₇H₁₇N₃O₃S

: 107-19-7
propargyl alcohol

: 1338831-30-3
{1-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-1,2,3-triazol-4-yl}methanol

Guidance literature:: C₁₇H₁₇N₃O₃S; With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

propargyl alcohol; With copper(l) iodide; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.09.004

Reference yield:

: 28798-81-4
(1-benzyl-[1,2,3]triazol-4-yl)methanol

: 1338831-30-3
{1-[(1-benzyl-1H-1,2,3-triazol-4-yl)methyl]-1H-1,2,3-triazol-4-yl}methanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With sodium azide; potassium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.09.004