(S)-N-benzyloxy-tbutyl-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester

Base Information

Chemical Name:(S)-N-benzyloxy-tbutyl-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester
CAS No.:229182-07-4
Molecular Formula:C₂₀H₂₅NO₇
Molecular Weight:391.421
Hs Code.:

Synonyms:(S)-N-benzyloxy-tbutyl-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester

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Chemical Property of (S)-N-benzyloxy-tbutyl-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester

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Technology Process of (S)-N-benzyloxy-tbutyl-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester

There total 3 articles about (S)-N-benzyloxy-tbutyl-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 229182-01-8
(S)-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester

: 229182-07-4
(S)-N-benzyloxy-tbutyl-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester

Guidance literature:: With dmap; In tetrahydrofuran; for 1h; Heating;
DOI:10.1016/S0040-4020(99)00267-7

Reference yield:

: 611-71-2
(R)-Mandelic Acid

: 229182-07-4
(S)-N-benzyloxy-tbutyl-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / BF₃*Et₂O / 1 h / Heating

2: 1.49 g / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 6 h

3: 95 percent / 4-(dimethylamino)pyridine / tetrahydrofuran / 1 h / Heating

With dmap; boron trifluoride diethyl etherate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1: Esterification / 2: Mitsunobu reaction / 3: Acylation;
DOI:10.1016/S0040-4020(99)00267-7

Reference yield:

: 10606-72-1
(R)-mandelic acid ethyl ester

: 229182-07-4
(S)-N-benzyloxy-tbutyl-2-acetamidoacrylic ethoxycarbonyl-phenyl-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.49 g / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 6 h

2: 95 percent / 4-(dimethylamino)pyridine / tetrahydrofuran / 1 h / Heating

With dmap; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1: Mitsunobu reaction / 2: Acylation;
DOI:10.1016/S0040-4020(99)00267-7