5-Bromo-3'-decyl-2,2':5',2''-terthiophene

Base Information

Chemical Name:5-Bromo-3'-decyl-2,2':5',2''-terthiophene
CAS No.:477335-02-7
Molecular Formula:C₂₂H₂₇BrS₃
Molecular Weight:467.558
Hs Code.:2934999090
DSSTox Substance ID:DTXSID90395154
Wikidata:Q82195045
Mol file:477335-02-7.mol

Synonyms:477335-02-7;5-bromo-3'-decyl-2,2':5',2''-terthiophene;2-(5-bromothiophen-2-yl)-3-decyl-5-thiophen-2-ylthiophene;5-BROMO-3'-DECYL-2,2';DTXSID90395154;AKOS015835606;FT-0677009;2,2':5',2''-Terthiophene,5-bromo-3'-decyl-

Suppliers and Price of 5-Bromo-3'-decyl-2,2':5',2''-terthiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
5-Bromo-3'-decyl-2,2':5',2''-terthiophene 95%
25mg
$ 312.00

American Custom Chemicals Corporation
5-BROMO-3'-DECYL-2,2':5',2''-TERTHIOPHENE 95.00%
25MG
$ 586.95

AK Scientific
5-Bromo-3'-decyl-2,2':5',2''-terthiophene
25mg
$ 471.00

Total 12 raw suppliers

Chemical Property of 5-Bromo-3'-decyl-2,2':5',2''-terthiophene

Chemical Property:

Boiling Point:508 °C at 760 mmHg
Flash Point:261 °C
PSA：84.72000
Density:1.265 g/cm³
LogP:9.65080
XLogP3:10.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:11
Exact Mass:466.04583
Heavy Atom Count:26
Complexity:392

Purity/Quality:

98%min ^*data from raw suppliers

5-Bromo-3'-decyl-2,2':5',2''-terthiophene 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCC1=C(SC(=C1)C2=CC=CS2)C3=CC=C(S3)Br

Technology Process of 5-Bromo-3'-decyl-2,2':5',2''-terthiophene

There total 4 articles about 5-Bromo-3'-decyl-2,2':5',2''-terthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 477335-01-6
1-(5-bromothien-2-yl)-2-decyl-4-thien-2-ylbutane-1,4-dione

: 477335-02-7
5-bromo-3'-decyl[2,2';5',2'']terthiophene

Guidance literature:: With hexamethyldisilathiane; boron trichloride; In hexane; toluene; at 20 ℃; for 1h;
DOI:10.1055/s-2002-32543

Reference yield:

: 112-16-3
n-dodecanoyl chloride

: 477335-02-7
5-bromo-3'-decyl[2,2';5',2'']terthiophene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 100 percent / AlCl₃ / benzene / 0.5 h / Heating

2.1: 100 percent / Br₂ / CH₂Cl₂ / 0.75 h / Heating

3.1: MeMgBr; Et₂NH / toluene / 3 h / 0 °C

3.2: 63 percent / Et₃N / toluene / 20 °C

4.1: 51 percent / hexamethyldisilathiane; BCl₃ / toluene; hexane / 1 h / 20 °C

With aluminium trichloride; hexamethyldisilathiane; methylmagnesium bromide; bromine; boron trichloride; diethylamine; In hexane; dichloromethane; toluene; benzene;
DOI:10.1055/s-2002-32543

Reference yield:

: 477334-99-9
1-(5-bromothien-2-yl)-dodecan-1-one

: 477335-02-7
5-bromo-3'-decyl[2,2';5',2'']terthiophene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 100 percent / Br₂ / CH₂Cl₂ / 0.75 h / Heating

2.1: MeMgBr; Et₂NH / toluene / 3 h / 0 °C

2.2: 63 percent / Et₃N / toluene / 20 °C

3.1: 51 percent / hexamethyldisilathiane; BCl₃ / toluene; hexane / 1 h / 20 °C

With hexamethyldisilathiane; methylmagnesium bromide; bromine; boron trichloride; diethylamine; In hexane; dichloromethane; toluene;
DOI:10.1055/s-2002-32543