methyl-2-(4-nitrophenyl)-1-phenylhydrazine

Base Information

• Chemical Name: methyl-2-(4-nitrophenyl)-1-phenylhydrazine
• CAS No.: 117911-80-5
• Molecular Formula: C₁₃H₁₃N₃O₂
• Molecular Weight: 243.265
• Mol file: 117911-80-5.mol

Synonyms:methyl-2-(4-nitrophenyl)-1-phenylhydrazine

Chemical Property of methyl-2-(4-nitrophenyl)-1-phenylhydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl-2-(4-nitrophenyl)-1-phenylhydrazine

There total 3 articles about methyl-2-(4-nitrophenyl)-1-phenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C18H15N2O4P (117911-73-6) + N-methylaniline (100-61-8) → methyl-2-(4-nitrophenyl)-1-phenylhydrazine (117911-80-5)

Guidance literature:

In tetrahydrofuran; at -10 ℃;

DOI:10.1016/S0040-4039(00)82041-9

Reference yield: 89.0%

para-dinitrobenzene (100-25-4) + N-methylaniline (100-61-8) → methyl-2-(4-nitrophenyl)-1-phenylhydrazine (117911-80-5)

Guidance literature:

With (1s,3s)-1,2,2,3,4,4-hexamethylphosphetane 1-oxide; mesitylenecarboxylic acid; diphenylsilane; In tetrahydrofuran; at 80 ℃; for 36h; chemoselective reaction; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1021/jacs.1c07272

Reference yield:

C18H14N2O4P(1-)*K(1+) (117911-82-7) → methyl-2-(4-nitrophenyl)-1-phenylhydrazine (117911-80-5)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl

2: 95 percent / tetrahydrofuran / -10 °C

With hydrogenchloride; In tetrahydrofuran;

DOI:10.1016/S0040-4039(00)82041-9

upstream raw materials:

C₁₈H₁₅N₂O₄P

N-methylaniline

C₁₈H₁₄N₂O₄P^(1-)*K⁽¹⁺⁾

para-dinitrobenzene