(Z)-1-Ethylidene-1,2,3,4-tetrahydro-6-methoxy-2-(3-methoxybenzoyl)-3-methylisoquinoline

Base Information

Chemical Name:(Z)-1-Ethylidene-1,2,3,4-tetrahydro-6-methoxy-2-(3-methoxybenzoyl)-3-methylisoquinoline
CAS No.:112649-86-2
Molecular Formula:C₂₁H₂₃NO₃
Molecular Weight:337.419
Hs Code.:

Synonyms:(Z)-1-Ethylidene-1,2,3,4-tetrahydro-6-methoxy-2-(3-methoxybenzoyl)-3-methylisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-Ethylidene-1,2,3,4-tetrahydro-6-methoxy-2-(3-methoxybenzoyl)-3-methylisoquinoline

Chemical Property:

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Technology Process of (Z)-1-Ethylidene-1,2,3,4-tetrahydro-6-methoxy-2-(3-methoxybenzoyl)-3-methylisoquinoline

There total 5 articles about (Z)-1-Ethylidene-1,2,3,4-tetrahydro-6-methoxy-2-(3-methoxybenzoyl)-3-methylisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1711-05-3
m-anisoyl chloride

: 112649-83-9
1-Ethyl-3,4-dihydro-6-methoxy-3-methylisoquinoline

: 112649-86-2
(Z)-1-Ethylidene-1,2,3,4-tetrahydro-6-methoxy-2-(3-methoxybenzoyl)-3-methylisoquinoline

Guidance literature:: With triethylamine; In benzene; for 0.5h; Ambient temperature;
DOI:10.1002/ardp.19873200905

Reference yield:

: 17862-85-0
3-methoxyamphetamine

: 112649-86-2
(Z)-1-Ethylidene-1,2,3,4-tetrahydro-6-methoxy-2-(3-methoxybenzoyl)-3-methylisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / pyridine / Ambient temperature

2: 55 percent / POCl₃ / acetonitrile / 3 h / Heating

3: 80 percent / Et₃N / benzene / 0.5 h / Ambient temperature

With pyridine; triethylamine; trichlorophosphate; In acetonitrile; benzene;
DOI:10.1002/ardp.19873200905

Reference yield:

: 134062-32-1
(E)-1-methoxy-3-(2-nitroprop-1-en-1-yl)benzene

: 112649-86-2
(Z)-1-Ethylidene-1,2,3,4-tetrahydro-6-methoxy-2-(3-methoxybenzoyl)-3-methylisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 45 percent / LiAlH₄ / diethyl ether / 1.5 h / Heating

2: 75 percent / pyridine / Ambient temperature

3: 55 percent / POCl₃ / acetonitrile / 3 h / Heating

4: 80 percent / Et₃N / benzene / 0.5 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; triethylamine; trichlorophosphate; In diethyl ether; acetonitrile; benzene;
DOI:10.1002/ardp.19873200905