1,2-anhydro-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

Base Information

Chemical Name:1,2-anhydro-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol
CAS No.:84218-82-6
Molecular Formula:C₆₄H₆₈O₁₂
Molecular Weight:1029.24
Hs Code.:

Synonyms:1,2-anhydro-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

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Chemical Property of 1,2-anhydro-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

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Technology Process of 1,2-anhydro-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

There total 17 articles about 1,2-anhydro-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1-O-p-toluenesulfonyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

: 84218-82-6
1,2-anhydro-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

Guidance literature:: With sodium methylate; In methanol; at 0 - 5 ℃; for 4h;

Reference yield:

: 84218-80-4
3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

: 84218-82-6
1,2-anhydro-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 72.2 percent / 4-dimethylaminopyridine / pyridine / 16 h / 0 - 5 °C

2: 85 percent / 0.5 N sodium methoxide / methanol / 4 h / 0 - 5 °C

With dmap; sodium methylate; In pyridine; methanol;

Reference yield:

: 84218-79-1,108867-18-1
1,2-O-cyclohexylidene-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

: 84218-82-6
1,2-anhydro-3-O-<2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranosyl>-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: 87.2 percent / p-toluenesulfonic acid / methanol / 16 h / 20 °C

2: 72.2 percent / 4-dimethylaminopyridine / pyridine / 16 h / 0 - 5 °C

3: 85 percent / 0.5 N sodium methoxide / methanol / 4 h / 0 - 5 °C

With dmap; sodium methylate; toluene-4-sulfonic acid; In pyridine; methanol;