methyl (E)-3-(4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazol-5-yl)-2-propenate

Base Information

• Chemical Name: methyl (E)-3-(4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazol-5-yl)-2-propenate
• CAS No.: 279252-28-7
• Molecular Formula: C₁₅H₁₃Cl₂IN₂O₂
• Molecular Weight: 451.091

Synonyms:methyl (E)-3-(4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazol-5-yl)-2-propenate

Chemical Property of methyl (E)-3-(4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazol-5-yl)-2-propenate

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Technology Process of methyl (E)-3-(4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazol-5-yl)-2-propenate

There total 1 articles about methyl (E)-3-(4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazol-5-yl)-2-propenate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazole-5-carbaldehyde (279252-27-6) + methyl (triphenylphosphoranylidene)acetate (21204-67-1,2605-67-6) → methyl (E)-3-(4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazol-5-yl)-2-propenate (279252-28-7)

Guidance literature:

In tetrahydrofuran;

Reference yield:

fur-2-ylboronic acid (13331-23-2) + methyl (E)-3-(4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazol-5-yl)-2-propenate (279252-28-7) + potassium carbonate (584-08-7) → methyl (E)-3-(4-chloro-1-(2-chloro-4-(2-furyl)benzyl)-2-methylimidazol-5-yl)-2-propenate (279252-29-8)

Guidance literature:

tetrakis(triphenylphosphine)palladium ⁽⁰⁾; In chloroform; water; N,N-dimethyl-formamide;

Reference yield:

methyl (E)-3-(4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazol-5-yl)-2-propenate (279252-28-7) → methyl (E)-3-(4-chloro-1-(2-chloro-4-((cyclopentyl)methyloxy)benzyl)-2-methylimidazol-5-yl)-2-propenate (279252-52-7)

Guidance literature:

upstream raw materials:

4-chloro-1-(2-chloro-4-iodobenzyl)-2-methylimidazole-5-carbaldehyde

methyl (triphenylphosphoranylidene)acetate

Downstream raw materials:

methyl (E)-3-(4-chloro-1-(2-chloro-4-(2-furyl)benzyl)-2-methylimidazol-5-yl)-2-propenate

methyl (E)-3-(1-(4-bromo-2-chlorobenzyl)-4-chloro-2-methylimidazol-5-yl)-2-propenate

methyl (E)-3-[4-chloro-1-(2-chloro-4-phenylbenzyl)-2-methylimidazol-5-yl]-2-propenate

methyl (E)-3-(4-chloro-1-(2-chloro-4-(1-propoxy)benzyl)-2-methylimidazol-5-yl)-2-propenate

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