methyl 3-acetamido-4-(1-acetyl-3-tert-butyl-1H-pyrazol-5-ylamino)benzoate

Base Information

Chemical Name:methyl 3-acetamido-4-(1-acetyl-3-tert-butyl-1H-pyrazol-5-ylamino)benzoate
CAS No.:1334849-38-5
Molecular Formula:C₁₉H₂₄N₄O₄
Molecular Weight:372.424
Hs Code.:

Synonyms:methyl 3-acetamido-4-(1-acetyl-3-tert-butyl-1H-pyrazol-5-ylamino)benzoate

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Chemical Property of methyl 3-acetamido-4-(1-acetyl-3-tert-butyl-1H-pyrazol-5-ylamino)benzoate

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Technology Process of methyl 3-acetamido-4-(1-acetyl-3-tert-butyl-1H-pyrazol-5-ylamino)benzoate

There total 5 articles about methyl 3-acetamido-4-(1-acetyl-3-tert-butyl-1H-pyrazol-5-ylamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82560-12-1,1237537-54-0
3-tert-butyl-1H-pyrazole-5-amine

: 1334849-38-5
methyl 3-acetamido-4-(1-acetyl-3-tert-butyl-1H-pyrazol-5-ylamino)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / 2 h / 20 °C

2: hydrazine hydrate / methanol / 1 h / Reflux

3: 0.08 h / 45 °C

With hydrazine hydrate; In methanol; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2011.06.006

Reference yield:

: 1020210-39-2,1304789-08-9
methyl 4-[(3-tert-butyl-1H-pyrazol-5-yl)amino]-3-nitrobenzoate

: 1334849-38-5
methyl 3-acetamido-4-(1-acetyl-3-tert-butyl-1H-pyrazol-5-ylamino)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 1 h / Reflux

2: 0.08 h / 45 °C

With hydrazine hydrate; In methanol;
DOI:10.1016/j.ejmech.2011.06.006

Reference yield:

: 453-71-4
3-nitro-4-fluorobenzoic acid

: 1334849-38-5
methyl 3-acetamido-4-(1-acetyl-3-tert-butyl-1H-pyrazol-5-ylamino)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 2 h / Reflux

2: dimethyl sulfoxide / 2 h / 20 °C

3: hydrazine hydrate / methanol / 1 h / Reflux

4: 0.08 h / 45 °C

With sulfuric acid; hydrazine hydrate; In methanol; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2011.06.006