phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside
CAS No.:952101-71-2
Molecular Formula:C₅₄H₇₉N₂O₉PSi₂
Molecular Weight:987.374
Hs Code.:

phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Synonyms:phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Suppliers and Price of phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

There total 6 articles about phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 952101-70-1
C₄₅H₆₂O₈Si₂

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 952101-71-2
phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/ejoc.200700203

Reference yield:

: 952101-68-7
C₃₁H₄₈O₆Si₂

: 952101-71-2
phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / TFA / CH₂Cl₂; H₂O / 4 h / 0 °C

2: 92 percent / pyridine / 12 h / 20 °C

3: 90 percent / DIEA / CH₂Cl₂ / 1 h / 20 °C

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In pyridine; dichloromethane; water;
DOI:10.1002/ejoc.200700203

Reference yield:

: 952101-69-8
C₂₄H₄₄O₆Si₂

: 952101-71-2
phenyl 4-O-[(2-cyanoethoxy)(diisopropylamino)phosphanyl]-6-O-(4,4'-dimethoxytriphenylmethyl)-2,3-di-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 12 h / 20 °C

2: 90 percent / DIEA / CH₂Cl₂ / 1 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In pyridine; dichloromethane;
DOI:10.1002/ejoc.200700203