1,2-xylenedioic acid 1-[6-[(3β,23-diacetoxylup-20(29)-en-28-oyl)oxy]hexyl] ester

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Chemical Name:1,2-xylenedioic acid 1-[6-[(3β,23-diacetoxylup-20(29)-en-28-oyl)oxy]hexyl] ester
CAS No.:1204202-45-8
Molecular Formula:C₄₈H₆₈O₁₀
Molecular Weight:805.062
Hs Code.:

Synonyms:1,2-xylenedioic acid 1-[6-[(3β,23-diacetoxylup-20(29)-en-28-oyl)oxy]hexyl] ester

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Chemical Property of 1,2-xylenedioic acid 1-[6-[(3β,23-diacetoxylup-20(29)-en-28-oyl)oxy]hexyl] ester

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Technology Process of 1,2-xylenedioic acid 1-[6-[(3β,23-diacetoxylup-20(29)-en-28-oyl)oxy]hexyl] ester

There total 4 articles about 1,2-xylenedioic acid 1-[6-[(3β,23-diacetoxylup-20(29)-en-28-oyl)oxy]hexyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 916139-80-5
9-acetoxy-8-acetoxymethyl-1-isopropenyl-5a,5b,8,11a-tetramethyl-eicosahydro-cyclopenta[a]chrysene-3a-carboxylic acid 6-hydroxy-hexyl ester

: 85-44-9
phthalic anhydride

: 1204202-45-8
1,2-xylenedioic acid 1-[6-[(3β,23-diacetoxylup-20(29)-en-28-oyl)oxy]hexyl] ester

Guidance literature:: 9-acetoxy-8-acetoxymethyl-1-isopropenyl-5a,5b,8,11a-tetramethyl-eicosahydro-cyclopenta[a]chrysene-3a-carboxylic acid 6-hydroxy-hexyl ester; phthalic anhydride; With dmap; In dichloromethane; at 20 ℃; for 10h;

With hydrogenchloride; In dichloromethane; water;
DOI:10.3390/molecules17088832

Reference yield:

: 85999-40-2
23-hydroxybetulinic acid

: 1204202-45-8
1,2-xylenedioic acid 1-[6-[(3β,23-diacetoxylup-20(29)-en-28-oyl)oxy]hexyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 20 °C

2: oxalyl dichloride / dichloromethane / 4 h / 20 °C

3: dichloromethane / 8 h / 20 °C

4: dmap / dichloromethane / 10 h / 20 °C

With pyridine; dmap; oxalyl dichloride; In dichloromethane;
DOI:10.3390/molecules17088832

Reference yield:

: 85999-41-3
3,23-diacetoxylup-20⁽²⁹⁾-en-28-oic acid

: 1204202-45-8
1,2-xylenedioic acid 1-[6-[(3β,23-diacetoxylup-20(29)-en-28-oyl)oxy]hexyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / dichloromethane / 4 h / 20 °C

2: dichloromethane / 8 h / 20 °C

3: dmap / dichloromethane / 10 h / 20 °C

With dmap; oxalyl dichloride; In dichloromethane;
DOI:10.3390/molecules17088832