(S,S)-1-[1-benzyl-3-(1-benzyl-2,2-dimethoxyethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide

Base Information

Chemical Name:(S,S)-1-[1-benzyl-3-(1-benzyl-2,2-dimethoxyethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide
CAS No.:1166398-94-2
Molecular Formula:C₂₈H₄₀N₄O₄
Molecular Weight:496.65
Hs Code.:

Synonyms:(S,S)-1-[1-benzyl-3-(1-benzyl-2,2-dimethoxyethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide

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Chemical Property of (S,S)-1-[1-benzyl-3-(1-benzyl-2,2-dimethoxyethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide

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Technology Process of (S,S)-1-[1-benzyl-3-(1-benzyl-2,2-dimethoxyethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide

There total 1 articles about (S,S)-1-[1-benzyl-3-(1-benzyl-2,2-dimethoxyethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1044510-13-5
(S)-imidazole-1-carboxylic acid (1-benzyl-2,2-dimethoxyethyl)amide

: 1166398-92-0
(S)-1-benzylaminopyrrolidine-2-carboxylic acid tert-butylamide

: 1166398-94-2
(S,S)-1-[1-benzyl-3-(1-benzyl-2,2-dimethoxyethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide

Guidance literature:: (S)-imidazole-1-carboxylic acid (1-benzyl-2,2-dimethoxyethyl)amide; With methyl iodide; In acetonitrile; at 20 ℃; for 12h; Inert atmosphere;

(S)-1-benzylaminopyrrolidine-2-carboxylic acid tert-butylamide; With triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmc.2009.03.059

Reference yield: 83.0%

: 1166398-94-2
(S,S)-1-[1-benzyl-3-(1-benzyl-2,2-dimethoxyethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide

: 1166398-96-4
(S,S)-1-[1-benzyl-3-(1-benzyl-2-oxoethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide

Guidance literature:: (S,S)-1-[1-benzyl-3-(1-benzyl-2,2-dimethoxyethyl)ureido]pyrrolidine-2-carboxylic acid tert-butylamide; With chloro-trimethyl-silane; sodium iodide; In acetonitrile; at 20 ℃; for 1h; Inert atmosphere;

With water; sodium hydrogencarbonate; In acetonitrile;
DOI:10.1016/j.bmc.2009.03.059