ethyl 3-(4-(N-methyl-N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)aminoethoxy)phenyl)-2-ethoxypropionate

Base Information

• Chemical Name: ethyl 3-(4-(N-methyl-N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)aminoethoxy)phenyl)-2-ethoxypropionate
• CAS No.: 264881-88-1
• Molecular Formula: C₃₁H₃₇NO₄
• Molecular Weight: 487.639

Synonyms:ethyl 3-(4-(N-methyl-N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)aminoethoxy)phenyl)-2-ethoxypropionate

Chemical Property of ethyl 3-(4-(N-methyl-N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)aminoethoxy)phenyl)-2-ethoxypropionate

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Technology Process of ethyl 3-(4-(N-methyl-N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)aminoethoxy)phenyl)-2-ethoxypropionate

There total 1 articles about ethyl 3-(4-(N-methyl-N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)aminoethoxy)phenyl)-2-ethoxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

ethyl 2-ethoxy-3-[4-(2-bromoethoxy)-phenyl]propanoate (220746-98-5) + N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-N-methylamine hydrochloride → ethyl 3-(4-(N-methyl-N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)aminoethoxy)phenyl)-2-ethoxypropionate (264881-88-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 5h;

DOI:10.1021/jm010964g

Reference yield:

ethyl 3-(4-(N-methyl-N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)aminoethoxy)phenyl)-2-ethoxypropionate (264881-88-1) → 3-(4-[2-([10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl]-methyl-amino)-ethoxy]-phenyl)-2-ethoxypropanoic acid

Guidance literature:

With hydrogenchloride; sodium hydroxide; acetic acid; In diethyl ether; ethanol; water; acetone;

Reference yield:

ethyl 3-(4-(N-methyl-N-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)aminoethoxy)phenyl)-2-ethoxypropionate (264881-88-1) → 3-(4-{2-[(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-methyl-amino]-ethoxy}-phenyl)-2-ethoxy-propionic acid

Guidance literature:

With sodium hydroxide; In ethanol; for 144h;

DOI:10.1021/jm010964g

upstream raw materials:

ethyl 2-ethoxy-3-[4-(2-bromoethoxy)-phenyl]propanoate

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