C₂₂H₂₂N₂O₅

Base Information

Chemical Name:C₂₂H₂₂N₂O₅
CAS No.:1616341-81-1
Molecular Formula:C₂₂H₂₂N₂O₅
Molecular Weight:394.427
Hs Code.:

C<sub>22</sub>H<sub>22</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₂H₂₂N₂O₅

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Chemical Property of C₂₂H₂₂N₂O₅

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Technology Process of C₂₂H₂₂N₂O₅

There total 13 articles about C₂₂H₂₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616341-78-6
C₂₄H₂₆N₂O₅

: 1616341-81-1
C₂₂H₂₂N₂O₅

Guidance literature:: With ethanol; potassium hydroxide; In tetrahydrofuran; at 20 ℃; for 0.5h;

Reference yield:

: 851389-58-7
2-tert-butyl 3-methyl (1R,3S,4S,6R)-6-hydroxy-2-azabicyclo[2.2.1]heptane-2,3-dicarboxylate

: 1616341-81-1
C₂₂H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

2.1: tetrahydrofuran; toluene / 2.5 h / 0 - 20 °C

3.1: hydrogen; hydrogenchloride; 20% palladium hydroxide-activated charcoal / ethanol / 0.5 h

4.1: lithium borohydride / tetrahydrofuran / 44 h / 0 - 35 °C

5.1: lithium borohydride; di-isopropyl azodicarboxylate / tetrahydrofuran / 19 h / 0 - 20 °C

6.1: hydrazine hydrate / ethanol / 1.5 h / 20 - 70 °C

7.1: sodium hydrogencarbonate / ethanol; water / 2 h / 20 °C

8.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1.5 h / 20 °C

8.2: 4.5 h / 100 °C

9.1: potassium hydroxide; ethanol / tetrahydrofuran / 0.5 h / 20 °C

With hydrogenchloride; lithium borohydride; ethanol; di-isopropyl azodicarboxylate; 20% palladium hydroxide-activated charcoal; hydrogen; sodium hydrogencarbonate; Dess-Martin periodane; hydrazine hydrate; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; toluene;

Reference yield:

: 1616341-73-1
C₁₃H₁₉NO₅

: 1616341-81-1
C₂₂H₂₂N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran; toluene / 2.5 h / 0 - 20 °C

2.1: hydrogen; hydrogenchloride; 20% palladium hydroxide-activated charcoal / ethanol / 0.5 h

3.1: lithium borohydride / tetrahydrofuran / 44 h / 0 - 35 °C

4.1: lithium borohydride; di-isopropyl azodicarboxylate / tetrahydrofuran / 19 h / 0 - 20 °C

5.1: hydrazine hydrate / ethanol / 1.5 h / 20 - 70 °C

6.1: sodium hydrogencarbonate / ethanol; water / 2 h / 20 °C

7.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1.5 h / 20 °C

7.2: 4.5 h / 100 °C

8.1: potassium hydroxide; ethanol / tetrahydrofuran / 0.5 h / 20 °C

With hydrogenchloride; lithium borohydride; ethanol; di-isopropyl azodicarboxylate; 20% palladium hydroxide-activated charcoal; hydrogen; sodium hydrogencarbonate; hydrazine hydrate; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; toluene;