3-METHYLBUTYRALDEHYDE-2,2-D2

Base Information

• Chemical Name: 3-METHYLBUTYRALDEHYDE-2,2-D2
• CAS No.: 352431-47-1
• Molecular Formula: C₅H₁₀O
• Molecular Weight: 89.11
• Mol file: 352431-47-1.mol

Synonyms:3-METHYLBUTYRALDEHYDE-2,2-D2;3-Methylbutanal(2,2-D2);Isovaleraldehyde(2,2-D2)

Chemical Property of 3-METHYLBUTYRALDEHYDE-2,2-D2

Chemical Property:

• Vapor Pressure: 49.3mmHg at 25°C
• Boiling Point: 93.5°Cat760mmHg
• Flash Point: °C
• PSA: 17.07000
• Density: 0.81g/cm³
• LogP: 1.23140

Purity/Quality:

99% ^*data from raw suppliers

3-Methylbutyraldehyde-2,2-d2 ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-Methylbutyraldehyde-2,2-d2 (CAS# 352431-47-1) is a useful isotopically labeled research compound.

Technology Process of 3-METHYLBUTYRALDEHYDE-2,2-D2

There total 3 articles about 3-METHYLBUTYRALDEHYDE-2,2-D2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isovaleraldehyde (590-86-3) → α,α-dideutero isovaleraldehyde (352431-47-1)

Guidance literature:

With sodium methylate; In d⁽⁴⁾-methanol; at 0 ℃; for 12h;

Reference yield:

3-methylbutanal-2,3-d2 → 3-methylbutanal-2,3,3-d3 (352431-47-1)

Guidance literature:

With pyridine; water-d2; at 130 ℃;

Reference yield:

3,3-dimethyl acrylaldehyde (107-86-8) → 3-methylbutanal-2,3,3-d3 (352431-47-1)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on activated charcoal; deuterium / water-d2 / 168 h / 20 °C

2: pyridine; water-d2 / 130 °C

With pyridine; palladium on activated charcoal; water-d2; deuterium; In water-d2;

upstream raw materials:

isovaleraldehyde

3,3-dimethyl acrylaldehyde