Trans-2,3,6,7,12,12a-hexahydro-2-benzyl-6-phenyl-pyrazino[2',1';6,1]pyrido[3,4-b]indole-1,4-dione

Base Information

Chemical Name:Trans-2,3,6,7,12,12a-hexahydro-2-benzyl-6-phenyl-pyrazino[2',1';6,1]pyrido[3,4-b]indole-1,4-dione
CAS No.:1224845-00-4
Molecular Formula:C₂₇H₂₃N₃O₂
Molecular Weight:421.499
Hs Code.:

Synonyms:Trans-2,3,6,7,12,12a-hexahydro-2-benzyl-6-phenyl-pyrazino[2',1';6,1]pyrido[3,4-b]indole-1,4-dione

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Chemical Property of Trans-2,3,6,7,12,12a-hexahydro-2-benzyl-6-phenyl-pyrazino[2',1';6,1]pyrido[3,4-b]indole-1,4-dione

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Technology Process of Trans-2,3,6,7,12,12a-hexahydro-2-benzyl-6-phenyl-pyrazino[2',1';6,1]pyrido[3,4-b]indole-1,4-dione

There total 5 articles about Trans-2,3,6,7,12,12a-hexahydro-2-benzyl-6-phenyl-pyrazino[2',1';6,1]pyrido[3,4-b]indole-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1447959-77-4
cis-ethyl 2-(2-chloroacetyl)-1-phenyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylate

: 100-46-9
benzylamine

: 1224845-00-4
Trans-2,3,6,7,12,12a-hexahydro-2-benzyl-6-phenyl-pyrazino[2',1';6,1]pyrido[3,4-b]indole-1,4-dione

Guidance literature:: In ethanol; at 20 ℃; for 24h;
DOI:10.1055/s-0032-1316911

Reference yield:

: 50302-60-8,50302-61-9,60702-94-5,60702-95-6,81089-84-1,91200-21-4,104330-95-2,111687-77-5
methyl 1-phenyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylate

: 100-46-9
benzylamine

: 1224845-00-4
Trans-2,3,6,7,12,12a-hexahydro-2-benzyl-6-phenyl-pyrazino[2',1';6,1]pyrido[3,4-b]indole-1,4-dione

Guidance literature:

Reference yield:

: 1227610-58-3
cis-1-phenyl-1,2,3,4-tetrahydro-9H-β-carboline-3-carboxylic acid ethyl ester

: 1224845-00-4
Trans-2,3,6,7,12,12a-hexahydro-2-benzyl-6-phenyl-pyrazino[2',1';6,1]pyrido[3,4-b]indole-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / ethyl acetate / 0.5 h / 0 °C

2: ethanol / 24 h / 20 °C

With sodium hydrogencarbonate; In ethanol; ethyl acetate;
DOI:10.1055/s-0032-1316911