Technology Process of C17H19BrN2O3
There total 4 articles about C17H19BrN2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C13H13BrN2O2;
With
N,O-bis-(trimethylsilyl)-acetamide;
In
acetonitrile;
for 0.25h;
bis(allyloxy)methane;
With
trimethylsilyl trifluoromethanesulfonate;
In
acetonitrile;
at 20 ℃;
for 30h;
Further stages.;
DOI:10.1002/ardp.200600163
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 88 percent / aq. chloroacetic acid / Heating
2.1: N,O-bis-(trimethylsilyl)acetamide / acetonitrile / 0.25 h
2.2: 35 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 30 h / 20 °C
With
N,O-bis-(trimethylsilyl)-acetamide; chloroacetic acid;
In
acetonitrile;
DOI:10.1002/ardp.200600163
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 58 percent / sodium ethoxide / ethanol / 8 h / Heating
2.1: 88 percent / aq. chloroacetic acid / Heating
3.1: N,O-bis-(trimethylsilyl)acetamide / acetonitrile / 0.25 h
3.2: 35 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 30 h / 20 °C
With
N,O-bis-(trimethylsilyl)-acetamide; sodium ethanolate; chloroacetic acid;
In
ethanol; acetonitrile;
DOI:10.1002/ardp.200600163