(1R,6S)-2-norcaranone cyclic (1S, 2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

Base Information

Chemical Name:(1R,6S)-2-norcaranone cyclic (1S, 2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal
CAS No.:99249-29-3
Molecular Formula:C₂₅H₃₀O₄
Molecular Weight:394.511
Hs Code.:

Synonyms:(1R,6S)-2-norcaranone cyclic (1S, 2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,6S)-2-norcaranone cyclic (1S, 2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

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Technology Process of (1R,6S)-2-norcaranone cyclic (1S, 2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

There total 6 articles about (1R,6S)-2-norcaranone cyclic (1S, 2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 99249-28-2
2-cyclohexen-1-one cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

: 99249-29-3,99295-87-1
C₂₅H₃₀O₄

Guidance literature:: With zinc copper; diiodomethane; iodine; potassium carbonate; In diethyl ether; for 24h; Heating;
DOI:10.1021/jo00281a044

Reference yield:

: 17401-06-8
(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol

: 99249-29-3
(1R,6S)-2-norcaranone cyclic (1S, 2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

3: zinc-copper couple, iodine / diethyl ether / 1 h / Heating

With zinc copper; iodine; In diethyl ether;
DOI:10.1021/ja00312a073

Reference yield:

: 75-11-6
diiodomethane

: 99249-28-2
2-cyclohexen-1-one cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

: 99249-29-3
(1R,6S)-2-norcaranone cyclic (1S, 2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

: 99295-87-1
C₂₅H₃₀O₄

Guidance literature:: With iodine; copper; potassium carbonate; zinc; In diethyl ether; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;
DOI:10.1021/jo00294a016