C₄₃H₆₆O₆Si₂

Base Information

Chemical Name:C₄₃H₆₆O₆Si₂
CAS No.:1443051-53-3
Molecular Formula:C₄₃H₆₆O₆Si₂
Molecular Weight:735.164
Hs Code.:

C<sub>43</sub>H<sub>66</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₄₃H₆₆O₆Si₂

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Chemical Property of C₄₃H₆₆O₆Si₂

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Technology Process of C₄₃H₆₆O₆Si₂

There total 10 articles about C₄₃H₆₆O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1443051-56-6
C₃₄H₄₈O₄Si

: 1443051-53-3
C₄₃H₆₆O₆Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: Dess-Martin periodane; sodium hydrogencarbonate / 0 °C

2: titanium tetrachloride; (-)-sparteine / dichloromethane / 2 h / 0 °C

3: 2,6-dimethylpyridine / dichloromethane

4: sodium tetrahydroborate / methanol / 3 h / 20 °C

5: Dess-Martin periodane / dichloromethane / 1 h

6: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tert-butyl alcohol; water

With 2,6-dimethylpyridine; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; titanium tetrachloride; sodium hydrogencarbonate; Dess-Martin periodane; (-)-sparteine; In methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2013.04.023

Reference yield:

: C₃₄H₄₆O₄Si

: 1443051-53-3
C₄₃H₆₆O₆Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: titanium tetrachloride; (-)-sparteine / dichloromethane / 2 h / 0 °C

2: 2,6-dimethylpyridine / dichloromethane

3: sodium tetrahydroborate / methanol / 3 h / 20 °C

4: Dess-Martin periodane / dichloromethane / 1 h

5: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tert-butyl alcohol; water

With 2,6-dimethylpyridine; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; titanium tetrachloride; Dess-Martin periodane; (-)-sparteine; In methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2013.04.023

Reference yield:

: 1443051-58-8
C₅₃H₇₅NO₅S₂Si₂

: 1443051-53-3
C₄₃H₆₆O₆Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 3 h / 20 °C

2: Dess-Martin periodane / dichloromethane / 1 h

3: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / tert-butyl alcohol; water

With sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; Dess-Martin periodane; In methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2013.04.023