tert-butyl 2-amino-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate

Base Information

Chemical Name:tert-butyl 2-amino-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate
CAS No.:936104-87-9
Molecular Formula:C₂₂H₃₄FNO₆S
Molecular Weight:459.579
Hs Code.:

Synonyms:tert-butyl 2-amino-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate

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Chemical Property of tert-butyl 2-amino-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate

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Technology Process of tert-butyl 2-amino-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate

There total 5 articles about tert-butyl 2-amino-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 936104-86-8
3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)-phenyl)-2,3-dihydroxy-propionate

: 936104-87-9
tert-butyl 2-amino-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate

Guidance literature:: Multistep reaction;
DOI:10.1016/j.tetlet.2007.01.085

Reference yield:

: 1033617-45-6
tert-butyl 2-azido-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate

: 936104-87-9
tert-butyl 2-amino-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 12h;
DOI:10.1016/j.bmc.2008.02.035

Reference yield:

: 2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethyl iodide

: 936104-87-9
tert-butyl 2-amino-3-(p-(2-(2-(tert-butoxycarbonylsulfanyl)ethoxy)ethoxy)phenyl)-3-fluoropropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / NaH / dimethylformamide

With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.01.085