m-hexyloxyphenylboronic acid

Base Information

• Chemical Name: m-hexyloxyphenylboronic acid
• CAS No.: 442686-90-0
• Molecular Formula: C₁₂H₁₉BO₃
• Molecular Weight: 222.092

Synonyms:m-hexyloxyphenylboronic acid

Chemical Property of m-hexyloxyphenylboronic acid

Chemical Property:

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Technology Process of m-hexyloxyphenylboronic acid

There total 3 articles about m-hexyloxyphenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-3-(hexyloxy)benzene (161291-04-9) → m-hexyloxyphenylboronic acid (442686-90-0)

Guidance literature:

1-bromo-3-(hexyloxy)benzene; With magnesium; In diethyl ether;

With Trimethyl borate; In diethyl ether;

With oxonium;

DOI:10.1039/b103450m

Reference yield:

1-bromo-hexane (111-25-1) → m-hexyloxyphenylboronic acid (442686-90-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: K₂CO₃ / ethanol / Heating

2.1: Mg / diethyl ether

2.2: B(OMe)3 / diethyl ether

2.3: H₃O⁺

With potassium carbonate; magnesium; In diethyl ether; ethanol;

DOI:10.1039/b103450m

Reference yield:

3-Bromophenol (591-20-8) → m-hexyloxyphenylboronic acid (442686-90-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: K₂CO₃ / ethanol / Heating

2.1: Mg / diethyl ether

2.2: B(OMe)3 / diethyl ether

2.3: H₃O⁺

With potassium carbonate; magnesium; In diethyl ether; ethanol;

DOI:10.1039/b103450m

upstream raw materials:

1-bromo-3-(hexyloxy)benzene

1-bromo-hexane

3-Bromophenol

Downstream raw materials:

(C₆H₁₃OC₆H₄)2C₆H₃BN₂H₂C₁₀H₆

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