2-Bromo-4-(tert-butyl)-5-methoxyaniline

Base Information

Chemical Name:2-Bromo-4-(tert-butyl)-5-methoxyaniline
CAS No.:1257834-30-2
Molecular Formula:C₁₁H₁₆BrNO
Molecular Weight:258.158
Hs Code.:
Mol file:1257834-30-2.mol

Synonyms:2-bromo-4-tert-butyl-5-methoxyphenylamine

Suppliers and Price of 2-Bromo-4-(tert-butyl)-5-methoxyaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Bromo-4-(tert-butyl)-5-methoxyaniline 95+%
5g
$ 842.00

Crysdot
2-Bromo-4-(tert-butyl)-5-methoxyaniline 95+%
1g
$ 326.00

Total 4 raw suppliers

Chemical Property of 2-Bromo-4-(tert-butyl)-5-methoxyaniline

Chemical Property:

Boiling Point:321.2±42.0 °C(Predicted)
PKA:2.44±0.10(Predicted)
Density:1.299±0.06 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

2-Bromo-4-(tert-butyl)-5-methoxyaniline 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Bromo-4-(tert-butyl)-5-methoxyaniline

There total 3 articles about 2-Bromo-4-(tert-butyl)-5-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 35291-89-5
4-tert-butyl-3-methoxyaniline

: 1257834-30-2
2-bromo-4-tert-butyl-5-methoxyphenylamine

Guidance literature:: With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/jm401329s

Reference yield:

: 79822-46-1
4-(1,1-dimethylethyl)-3-(methoxy)benzoic acid

: 1257834-30-2
2-bromo-4-tert-butyl-5-methoxyphenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: diphenylphosphoranyl azide; triethylamine / tetrahydrofuran / 23 h / Reflux; Inert atmosphere

2: potassium hydroxide; water / ethanol / 15 h / Reflux; Inert atmosphere

3: N-Bromosuccinimide / N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; diphenylphosphoranyl azide; water; triethylamine; potassium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 1: |Curtius Rearrangement;
DOI:10.1021/jm401329s

Reference yield:

: 1485748-67-1
ethyl N-(4-tert-butyl-3-methoxyphenyl)carbamate

: 1257834-30-2
2-bromo-4-tert-butyl-5-methoxyphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; water / ethanol / 15 h / Reflux; Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; water; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm401329s